GCMS analysis results for sample AD31664, Jan 25 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN22\31664.D Vial: 1 Acq On : 22 Jan 2002 2:41 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 METHYLFULVENE Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

4.37 0.07 ug/L 21004 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 METHYLFULVENE 92 C7H8 000000-00-0 9 2 1,3,5-Cycloheptatriene (CAS) $$ ... 92 C7H8 000544-25-2 9 3 ETHINYLCYCLOPENTENE-(1) 92 C7H8 000000-00-0 9 4 Cyclobutene, 2-propenylidene- 92 C7H8 052097-85-5 7 Abundance Scan 87 (4.367 min): 31664.D (-) m/z 91.10 100.00% SI

5000 * ■ i ■ ■ ■ ■ i ■ 39 51 65 84 4.00 4.20 4.40 4.60 4.80 1 m/z 92.10 52.73% miz-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5531: METHYLFULVENE 91

5000 4.00 4.20 4.40 4.60 4.80 m/z 65.10 9.54% 39 . 65 1 45 61 , ।, asrksssuth‘tos*ssi**"s*soa**1***[* 1 ■ i ■■ ■11' ■ niz-> 3035404550556065 70 75 808590 95 100 Abundance #5568:1,3,5-Cycloheptatriene (CAS) $$ Cycloheptatriene $$... 91 ■ • i ■ ■ • ' i ■ ■ • ■ i • ■ 1 ■ I 1 1 ■ • i ■ 4.00 4.20 4.40 4.60 4.80 5000 m/z 51.00 9.40%

miz-> Abundance 39 .1 .. ।. • • • । 65 61 , | 86 • 11 • • • • i ■ > • • k • • ■ • i ’ • ■ • i11' * I * • ■ • i •' • ■ i • • ■ • i • • ‘ • i * • ■ • l' 3035404550 55 6065 70 75808590 95 100 #5532: ETHINYLCYCLOPENTENE-(1) 91 i ■ j ■ • • • i • ■

MMYiyanh ' 1 I ' I ' ' I I I *1 I'[ 1 I / "rri r I I1 4.00 m/z 4.20 39.10 4.40 4.60 8.25% 4.80

5000

39 TIIWPTLTmImmputte 6165 1 ■ 111 • ■ i ■ ■ ■ ' i ■ ■ • ■ i ■ > • ■ i ■ • • ■ I ■ 1 1 ■ i ■ m/z—> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 4.00 4.20 4.40 4.60 4.80

31664.D SCAN508.M Thu Jan 24 14:00:06 2002 Page 4

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