GCMS analysis results for sample AE00103, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00103 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050384–000050396

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN23\00103.D Vial: 5 Acq On : 23 Jan 2002 6:15 pm Operator: .Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 METHYLFULVENE Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 4.38 0.12 ug/L 41538 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 METHYLFULVENE 92 C7H8 000000-00-0 9 2 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2 7 3 Spiro[2,4]hepta-4,6-diene $$ Spi... 92 C7H8 000765-46-8 7 4 1,3,5-Cycloheptatriene (CAS) $$ ... 92 C7H8 000544-25-2 7 Abundance Scan 88 (4.378 min): 00103.D (-) m/z 91.00 100.00% SI

5000

I*’**I+’11*+’’I’**’1** 65 4.00 4.20 4.40 4.60 4.80 39 50 86 , m/z 92.10 59.83% **GGG* "i■•••i1■•'i "i" •11 I “ “1 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5531: METHYLFULVENE sb

5000 ............... \_ ‘ i 1 ■ ■ ■ i ' ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ • i ■ 1 4.00 4.20 4.40 4.60 4.80 m/z 65.00 11.04% 39 65 I 45 61, ।, 0- ' ‘ I ' 1 ■ ‘ I ' ■ ‘ ' I' ttt | > I I I | 1 । | । | . . rfT ■ 1 rTt f I 11 I > l 1 | . . I : J i i i . | . I M | . I ■ I | Pmp niz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5569:1,3,5-Cycloheptatriene 91 ■ I ‘ ' I ■ ‘ I * ‘ ‘ • 1 * ' I l j * ‘ 4.00 4.20 4.40 4.60 4.80 5000 m/z 39.10 7.37% 65

miz—> 27 37 Of TI_mn—umuuNuatu]7 46 51 —1H+ ' l1 ■1 ■ i11 ■11"111 ■1'11 1’11111113 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5553: Spiro[2,4]hepta-4,6-diene $$ Spiro[2.4]hepta-4,6-diene ‘ I ' ‘ ‘ ' I ‘ ‘ ‘ I ‘ ‘ ‘ I ‘ * • * I ‘ * 91 4.00 4.20 4.40 4.60 4.80 m/z 89.10 5.10% 5000

65 '11 ■' ■' l ■ ■ ■' 51 01 '' I' ■ ■' l “'' I ■ ■'' I ■'39 1 111 ,1" 1 1 ■ ■ l' ■ ■ ■ 61, 77 ■ । ‘ ■ i ■ 11 NIPpo • i • > > « i < • i • ■ ■ ■ i ■ ■ ■ ■ i ■ • n/z—> 2025303540 45 50556065 70 75 80 85 90 95 100 4.00 4.20 4.40 4.60 4.80

00103.D SCAN508.M Thu Jan 24 09:57:18 2002 Page 4

NYC-WTC_000050391

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000050391Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS analysis results for sample AE00698, Jan 2002 · Box DEP Box 28

NYC-WTC_000050397

Laboratory report for sample AE00698 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

1 shared topics · Same agency, volume and box · similarity 0.998