GCMS analysis results for sample AE01637, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report . Data File : C: \MSDCHEM\1\5973N\02FEB21\01637.D Vial: 6 Acq On : 21 Feb 2002 7:22 pm Operator: Sample : 508 scan Inst : 1nstrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 4 METHYLFULVENE Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

4.39 0.05 ug/L 21662 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 METHYLFULVENE 92 C7H8 000000-00-0 7 2 1,3,5-Cycloheptatriene (CAS) $$ ... 92 C7H8 000544-25-2 7 3 1,3,5-Cycloheptatriene 92 C7H8 000544-25-2 4 4 Tricyclo[4.1.0.0(2,7)]hept-3-ene... 92 C7H8 035618-58-7 4 Abundance Scan 90 (4.390 min): 01637.D (-) m/z 91.00 100.00% 91

5000 43 51 65 85 ■ i ■ ■ 1 ■ i ■ 4.00 4.20 H 4.40 ’111’1’’ 4.60 4.80 0+ i■■■■i‘■i•■■ ■ i ■ ■ ■■ i i ■ ■" i i' •1 ■ i i**•■r -n-p-r-TTp-r m/z 92.10 67.79% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5531: METHYLFULVENE 91

5000 • !>><>!> I • i ■ ■ ■ ■ i ■ ■ 4.00 4.20 4.40 4.60 4.80 m/z 43.10 20.25% 39 1 45 61 . 651, 0 T1—*P)PTRTTWIIITTmH Pponput miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5568:1,3,5-Cycloheptatriene (CAS) $$ Cycloheptatriene $$... 91 4.00 4.20 4.40 4.60 4.80 5000 m/z 51.00 16.04% j 39 61 65 86 m/z-> Of 0 WInun]uBppp———mugmtt 1' । । 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5569:1,3,5-Cycloheptatriene i •1 ■ ■ i • ■ 91 4.00 4.20 4.40 4.60 4.80 m/z 65.00 14.77%

5000

65 27 37 46 51 61,| 0 ■ • I' ■ '' I ‘" I'' ' ‘ I ‘1 '' I'‘' 11 ' । ‘ |' • • ■ । ■ 1111 111 n ' i1 ■ ■ ■ i ■ “ ■ i "'11' — vrp-r-rrp-r 1 i 1 ' 1 1 i ■ ■ ■ ■ I 1 1 ' i 1 1 ' ' i ' ' miz—> 20253035 40 4550556065 70 75 80 85 90 95 100 4.00 4.20 4.40 4.60 4.80

01637.D HP022102.M Mon Feb 25 10:55:43 2002 Page 6

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