GCMS analysis results for sample AE01637, March 2002

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GCMS laboratory results for sample AE01637 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010106–000010125

Folder label: “GCMS X 1/23/02 A 2/21/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB21\01637.D Vial: 6 Acq On : 21 Feb 2002 7:22 pm Operator: .Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 l-Hexene, 4,5-dimethyl- $$ ... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

5.03 0.06 ug/L 29054 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 l-Hexene, 4,5-dimethyl- $$ 4,5-D... 112 C8H16 016106-59-5 28 2 Butanoic acid, 2-propenyl ester 128 C7H12O2 002051-78-7 25 3 Butanoic acid, 2-propenyl ester ... 128 C7H12O2 002051-78-7 25 4 Butanoic acid, 2-ethylhexyl ester 200 C12H2402 000000-00-0 25 Abundance Scan 147 (5.033 min): 01637.D (-) m/z 43.10 100.00% 43 71

59 5000

207 ,{.>4..^^..^. J... 4.60 4.80 5.00 5.20 5.40 01 — m/z 71.00 98.44% niz—> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #13811: 1-Hexene, 4,5-dimethyl- $$ 4,5-DimethyH-hexene 43 71

5000 55 AA5.40 4.60 4.80 5.00 5.20 27 m/z 41.10 86.97%

niz-> 0! .,. .1. Ia.r 4 84 97 h।...।.।i..I।।11.।..।.... 11... 11।। ____. ।।।।। 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #24321: Butanoic acid, 2-propenyl ester 43 71 4.60 ... W....... 4.80 5.00 5.20 5.40 5000 27 m/z 59.00 55.20%

i 57 , 89 100 128 0- ............... ....... 11 , .. T. ।. ।... .'|.... ।... 1111.... j।. ।.... ।.... ।.... ।.... ।.... ।... n/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #24319: Butanoic acid, 2-propenyl ester $$ Butyric acid, a... 43 71 4.60 4.80 5.00 5.20 5.40 m/z 55.10 35.58% 5000 27 57 , 89 100 0 mpt Irmm 'I... ।... .’|.... ।....... 11111.111... ।.... ।.... ।.... ।.... ।....(. ।.. ।.... ।.. । i ■ ■ ■ ■ i ■ ■ n/z—> 20 30 40 50 60 70 80 90 100110120130140150160170180190 200210 4.60 4.80 5.00 5.20 5.40

01637.D HP022102.M Mon Feb 25 10:55:44 2002 Page 7

NYC-WTC_000010116

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NYC-WTC_000010116Source: NYC Law Department, mirrored locally

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GCMS analysis report for sample AE01636, March 2002 · Box DEP Box 14

NYC-WTC_000010086

GCMS laboratory results for sample AE01636 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

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