GCMS analysis results for sample AE00105, Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02JAN25\00105.D Vial: 3 Acq On : 25 Jan 2002 11:49 am Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 6 l-Hexene, 4,5-dimethyl- $$ ... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 5.71 0.20 ug/L 83690 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 l-Hexene, 4,5-dimethyl- $$ 4,5-D... 112 C8H16 016106-59-5 64 2 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 49 3 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 47 4 Butanoic acid, 2-propenyl ester ... 128 C7H12O2 002051-78-7 43 Abundance Scan 205 (5.714 min): 00105.D (-) m/z 71.10 100.00% 43 71

5000 39

' ' I 1 ' ' ' I ' ■ • i > • • ■ । 53 58 67 84 5.40 5.60 5.80 600

m/z-> —l I................ Ml 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 11 ■ •' I ’ • ■' I ’ " ' I TT m/ z 43.10 87.84% Abundance #13811:1-Hexene, 4,5-dimethyl- $$ 4,5-Dimethyl-1-hexene 43 71

5000 39 55 5.40 5.60 5.80 6.00 27 m/z 41.10 86.22% 67 84 m/z-> -- ■ ■ r ''' i' ....... 97 M I" " I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 TT

Abundance #4085: 3-Buten-2-ol, 2-methyl- 43 7 -

5.40 5.60 5.80 6.00 5000 m/ z 39.10 45.75% 59 27 31 53 671 11।।■i । L ■■ -PH 86 1" r " ' i' " ' i1" ' i ■ " ' r ■ " i" " i ■ i" • ’ i r'" i n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #4084:3-Buten-2-ol, 2-methyl- 43 71 5.40 5.60 5.80 6.00 m/z 69.10 36.76% 5000 59

n/z-> mmmmm TI" 27 53 v । 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 67 86 i■•।■••■।>11।। ■ > • ■ । • ■ ■ • । • 5.40 .A. 5.60 5.80 6.00

30105.D SCAN508.M Mon Jan 28 09:49:48 2002 Page 8

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