GCMS analysis results for sample AE00105, Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN25\00105.D Vial: 3 Acq On : 25 Jan 2002 11:49 am Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 7 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 3.55 ug/L 1512160 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 220 (5.885 min): 00105.D (-) m/z 73.10 100.00% 73

5000 43 5.60 5.80 6.00 6.20 87 103 Tl/Z-> ....... 20 1555,... '.J '1' 11 v 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 i ■' ■ ■ i ■ ■ ■' i m/z 43.10 26.42% Abundance #36138: 3-(CYCLOHEX-3‘-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 5.60 5 80 6.00 6.20 43 m/z 45.10 9.48%

n/z-> 20 —2 30 40 55..... ,, 87 113 174 ........ ... " 'r' —— TIT ■ ■ i ■ ■ ■ ■ i''111'111 r111 r11 ■ i ■ ■ ■■i■11■r■■■i■ 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 7(3

5.60 5.80 6.00 6.20 5000 m/z 41.10 9.45% 43

■। 27 1,55. ..........11" 11 TT i > > > ■ i' 87 113 i• >•• i• •• >। > i>>•■ i > ■■ •i 174 l ■ ‘ ■ i ■ miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 - Abundance #4815: Silane, tetramethyl- 73 5.60 5.80 6.00 6.20 m/z 71.10 6.78% 5000

45 31 || 59 - 88 PTTT ’IT TT T‘ n/z-s 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

30105.D SCAN508.M Mon Jan 28 09:49:48 2002 Page 9

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