GCMS analysis results for sample AE00366, Jan 18 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00366 conducted on January 18, 2002.

NYC-WTC_000051236–000051251

Folder label: “GCMS X 1/8/02 A 1/10/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\O2 JAN10\00465.D Vial: 3 Acq On : 10 Jan 2002 4:28 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 4 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 5.20 ug/L 1646850 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 23 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 220 (5.885 min): 00465.D (-) m/z 73.10 100.00% 73

5000 43 5.60 5.80 6.00 6.20

m/z-> o1 —5 4..... "in T*IT TT । 87 103 I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' " ' I ' 1 ' ' I m/z 43.10 24.05% 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 7)3

5000 5.60 5.80 6.00 6.20 43 m/z 45.10 9.49% 27 55 174 87 113 m/z-> +711) 0- .................... '............. 'i1'1' ■ i • i' ■ ■' , ri TTTTT i11" r 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 i' ■ ’' i ■ ■ " i " '' i

Abundance #78238: Acetic acid, 3-[1 ,3]dioxolan-2-ylpropyl ester 73

5.60 5.80 6.00 6.20 5000 m/z 41.10 9.11% 43 27 87 oW i’”•i ... 1’ T+r 55 1 113 ■ i" " i " '' i' 174 i " " i " ' • i "'11 ■ ■ ■ ■ i " '' r ■ " i' " ' r ■ " i " ' ■ i ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4814: Silane, tetramethyl- 73 5.60 5.80 6.00 6.20 m/z 71.10 6.78% 5000

45 15 | 53 1 88 0 r'"r"'i | I I1! I | MI’lmil I1 1111"'11" " i | |' •' • " I ’ ’ ’ ' I i ■ ■ • ■«■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

)0465.D SCAN508.M Fri Jan 11 10:08:29 2002 Page 6

NYC-WTC_000051245

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NYC-WTC_000051245Source: NYC Law Department, mirrored locally

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