GCMS results for sample AE00315, Jan 24 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN14\00315.D Vial: 4 Acq On : 14 Jan 2002 12:59 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 14, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 3 3-(CYCLOHEX-3‘-EN-YL)PROPAN... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 3.65 ug/L 1333590 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

13-(CYCLOHEX-3‘-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 Silane, tetramethyl- (CAS) $$ Te... 88 C4H12Si 000075-76-3 9 Abundance Scan 220 (5.885 min): 00315.D (-) m/z 73.10 100.00% 73

5000 43 ) , .... 5.60 5.80 6.00 6.20 0 I ■ ■ i 4455. — 87 103 +0PPTTTTT T‘‘‘1011111 m/z 43.10 24.49% Tl/Z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3’-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

— _ __ 5000 5.60 5.80 6.00 6.20 43 m/z 45.10 9.49% 27 55 113 , 1 — 87 174 0 TTO ।.... i.... । i ■'1 ■ i Ti ■ ■ ■' i •' * ■ i ■ " ' i i ■ ■ i ■ ■'

rn/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-(1,3)dioxolan-2-ylpropyl ester 70 5.60 5.80 6.00 6.20 5000 m/z 41.10 9.29% 43 ..... .........

27 55 87 113 174 01 TT 11 ■1" i " ■ 'i' 'l ■■ I -p-TT i" ■ ■ i ■' •1 r ■' ■ i1' ■ ■ i l1 " ' I ’ n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... T-T-p-r-r-i- 30 5.60 5.80 6.00 6.20 73 m/z 71.10 6.46%

5000 44 58 15 Tl/Z-> 0 M 10 20 30 An- 50 60 70 80 90 100 110 120 130 140 150 160 170 180 40 - 5.60 5.80 6.00 6.20

00315.D SCAN508.M Tue Jan 15 08:47:54 2002 Page 5

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