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GCMS results for sample AE00315, Jan 24 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00315 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051380–000051393

Folder label: “GCMS X 1/8/02 A 1/11/02

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Scanned page image, NYC-WTC_000051389
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN14\00315.D Vial: 4 Acq On : 14 Jan 2002 12:59 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 14, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 2-Propanol, 1-(2-methoxypro. . . Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.

9.85 0.13 ug/L 45907 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 83 2 Butanoic acid, 2-hydroxy- $$ But... 104 C4H803 000565-70-8 9 3 Butane, 2-methoxy- (CAS) $$ Meth... 88 C5H120 006795-87-5 9 4 Butane, 2-methoxy- $$ Ether, sec... 88 C5H120 006795-87-5 9 Abundance Scan 567 (9.847 min): 00315.D (-) m/z 59.10 100.00% 59

5000 , MM.... 45 73

m/z-> 0 ■I■'■■l■■ ■ ■I■ L 10 20 30 40 50 60 70 80 90 100 110 120 104 130 m/z 9.60 45.10 9.80 10.00 10.20 14.89%

Abundance #43942:2-Propanol, 1-(2-methoxypropoxy)-$$ 1-(2-Methoxyp... 59

, — 5000 9.60 9.80 10.00 10.20 m/z 73.10 13.99% 31 45 I , ,l|i j,,,, ■ -111.... । 73 104 J....... . ■ ■ . Pl . 130 0 • i • • • • । > i • 1 r1 1 1 1 r1 rn/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #10063: Butanoic acid, 2-hydroxy- $$ Butyric acid, 2-hydro... 31 59 AAV /A ' I ' ' ' ' I ' ' ' ' I 9.60 9.80 10.00 10.20 5000 m/z 41.10 12.45% 45 76 A 0■■।■•>■। ■ ..... ... 'I... I 1 111 p 1 1 I |..... I..... . ........... , m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4937: Butane, 2-methoxy- (CAS) $$ Methyl sec-butyl ether... 59 9.60 9.80 10.00 10.20 m/z 43.10 9.95%

5000 A 15 27 73 45 0 . 1.. . — | 88 > > i ■ * ■ ■ i > > 1 > I > ■ 11 11 11 ITTTTT ■ i ■ ' ■ ' i ■ 1 ' ’ i 1 ■ ■ ■ I ' 1

/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 9.60 9.80 10.00 10.20

00315.D SCAN508.M Tue Jan 15 08:47:55 2002 Page 6

NYC-WTC_000051389

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