GCMS results for sample AE00315, Jan 24 2002

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Laboratory report showing GCMS analysis of sample AE00315 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051380–000051393

Folder label: “GCMS X 1/8/02 A 1/11/02”

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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\5973N\02JAN14\00315.D Vial: 4 Acq On : 14 Jan 2002 12:59 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 14, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 22.28 0.15 ug/L 94607 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 64 2 2,4-Diamino-6-(hydroxymethyl)pte... 192 C7H8N6O 000945-24-4 59 3 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 4 6-Methoxy-2,4-dihydroxy-1,5-naph... 192 C9H8N203 000000-00-0 50 Abundance Scan 1656 (22.280 min): 00315.D (-) m/z 192.10 100.00% 192

5000

89 96 'I6 160

n/z-> 0 42 66 82 nmmPPRHm P I 118 1 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 i' ” ■ i l. 22.00 22.20 22.40 22.60 m/z 146.10 16.13% Abundance #102588:4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

5000 108 A........) I ' ' ’ ' I ' ' ' I ‘ 22.00 22.20 22.40 22.60 146 175 m/z 191.10 15.43%

0 ‘‘I ‘‘‘‘I T‘t1111101017110"T7111T ।" " r "' i" • ■ । r ’ ‘ ■ i ■' " i 1’1111 n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102010:2,4-Diamino-6-(hydroxymethyl)pteridine 192 163 22.00 22.20 22.40 22.60 5000 m/z96.10 14.07%

66 146 175 0 34 " r 1 ■' i ■' " i " " i ............ 121.135 I—— L i " " r ■ u i1 • ” i " ■ ■ I " ” I' ”' i ■'1 ’T i‘ nlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192 22.00 22.20 22.40 22.60 m/z 193.10 12.45%

5000 82

54 110

/z-> 0 — 30 i" • ■ i • ■ • ■ i 94 160 11111" 111111"11111" I.....1111'1,11 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 U 22.00 22.20 22.40 22.60

00315.D SCAN508.M Tue Jan 15 08:47:55 2002 Page 7

NYC-WTC_000051390

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NYC-WTC_000051390Source: NYC Law Department, mirrored locally

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NYC-WTC_000051394

Laboratory report showing GCMS analysis of sample AE00321 with surrogate recovery data on January 24, 2002.

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