GCMS results for sample AE00315, Jan 24 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN14\00315.D Vial: 4 Acq On : 14 Jan 2002 12:59 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 14, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 6 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.34 ug/L 220865 Phenanthrene-dl 0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 87 2 Phenanthrene-diO 188 C14D10 001517-22-2 64 3 Acridine-D9 188 C13D9N 000000-00-0 59 4 Acridine-D9 188 C13D9N 000000-00-0 45 Abundance Scan 1699 (22.771 min): 00315.D (-) m/z 188.15 100.00% 188

5000 94 — 80 158 22.40 22.60 22.80 23.00 23.20

m/z-> Or—+ 40 52 66 I (■ >. 1. 11.! ■ ■ 11 m tilhasya i • • ■ • i 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 132 TP m/ z 94.10 25.58% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/Z 189.10 16.57% 66 n/z-> Oh rolusssassssyvolugua — । ■• ■ ■ । 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 5s...... lull... Abundance #84499: Phenanthrene-d10 188 ■ i ■ ’ ■ ' i • ' • r I ■ ■ ■ ■ i ■ ■ ■ ■ i ■ 22.40 22.60 22.80 23.00 23.20 5000 m/ z 80.00 13.30%

80 94 160 66 Or ■ i ■ ■ " i ■ - H r ' ■ ■ i ■ ■ " i " ■ ■ i' ■ ■' i III...... 19/... n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #85254: Acridine-D9 1(18 22.40 22.60 22.80 23'00 23'20 m/z 184.10 13.24%

5000

93 158

rn/z-> 66 80 || Oh " i " " i' " 1111111" " 111" rt1 111111111111'11' 1" •' 1 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ..... .J... 22.40 22.60 22.80 23.00 23.20

)0315.D SCAN508.M Tue Jan 15 08:47:55 2002 Page 8

NYC-WTC_000051391