GCMS results for sample AE00315, Jan 24 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN14\00315.D Vial: 4 Acq On : 14 Jan 2002 12:59 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 14, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Decanedioic acid, bis(2-eth... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 33.40 0.14 ug/L 74187 Perylene-dl2 34.42

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Decanedioic acid, bis(2-ethylhex... 426 C26H50O4 000122-62-3 59 2 dl-2-Ethylhexyl chloroformate $$... 192 C9H17C1O2 024468-13-1 35 3 8-Benzenesulphonyloxyquinoline 185 C12H11NO 000000-00-0 35 4 Dibutyl ester of decanedioic acid 314 C18H3404 000000-00-0 27 Abundance Scan 2630 (33.400 min): 00315.D (-) m/z 185.10 100.00% 185

57 5000 112 83 । 33.00 33.20 33.40 33.60 33.80 0 ,,Ti ■ I.... I" " I' ।" ‘* “I T*UIU‘U"TT‘‘t‘i m/z 57.10 63.37%

L n/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #345444: Decanedioic acid, bis(2-ethylhexyl) ester (CAS) S... 185 57

5000 112 i-r AAAMM 33.00 33.20 33.40 33.60 33.80 m/z 70.10 44.40% 426 0 TTT r "• i' ”11 |••■•| • l ” " I' " ■ l' 'I r ■ ”i" " i ’ I 11 m/z-> 40 60 80 100120140160180200220240260280 300320340 360380400420 Abundance #102311: dl-2-Ethylhexyl chloroformate $$ 2-Ethylhexyl chi... 57 112 33.00 33.20 33.40 33.60 33.80 5000 m/z 71.10 43.62% 83

.. .lb.... 148 192 O-pr Trp-rrTprrrp-rTTyTTTTp-rTTp-rrrpT-rTp-rTTTTTTTp-i^^ m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #94147:8-Benzenesulphonyloxyquinoline 57 185 33.00 33.20 33.40 33.60 33.80 m/z 55.10 34.23% 94 112 5000 167

/z-> 0 I" " 11"1 r "11" " 11"11"1111 ■ ■ ■ r "' I" " r " ■ r •" i 40 60 80 100120140160180200220240260280300320340360380400420 A I. M I • ■ • ■ I 33.00 33.20 33.40 33.60 33.80

00315.D SCAN508.M Tue Jan 15 08:47:55 2002 Page 9

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