GCMS results for sample AE00463, Jan 24 2002

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Laboratory report showing GCMS analysis of sample AE00463 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051422–000051438

Folder label: “GCMS X 1/8/02 A 1/11/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN11\00463.D Vial: 5 Acq On : 11 Jan 2002 5:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 10 Decanedioic acid, bis(2-eth... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 33.40 0.93 ug/L 434753 Perylene-dl2 34.42 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Decanedioic acid, bis(2-ethylhex... 426 C26H50O4 000122-62-3 43 2 2-Nonanol, 5-ethyl- (CAS) $$ 5-E... 172 C11H240 000103-08-2 43 3 2-cyanomethylene-3-oxo-l,2,3,4-t. .. 185 C10H7N3O 000000-00-0 40 4 Propanedioic acid, hexyl-, dieth... 244 C13H2404 005398-10-7 35 Abundance Scan 2630 (33.400 min): 00463.D (-) m/z 185.10 100.00% 185

57 5000 112 | 83 i • ' 1 ■ i ■ YPr

n/2-> 0- 4 L4 143 166 203 "i' "■ r"'i""r'1 ■ r"'r"■ r■ "i""i ""i"i" "i'“'i 40 60 80 100120140160180200220240260280300320340360380400420 33.00 33.20 33.40 33.60 33.80 m/ z 57.10 58.73% Abundance #345444: Decanedioic acid, bis(2-ethylhexy!) ester (CAS) $... 185 57 _ 112 5000 33.00 3320 33.40 33.60 33.80 m/z 70.10 39.49% 426

.. C 0 I ' "Yl " " I P'111"111"111111 ‘111" I"111"111"111" " r "' r"' r "'r '" i"" i" " i" •'i n/z-> 40 60 80 100120140160180200 220240260280300320340360380400420 Abundance #76872: 2-Nonanol, 5-ethyl- (CAS) $$ 5-Ethyl-2-nonanol $$ ... 57

33.00 33.20 33.40 33.60 33.80 5000 112 m/z 71.10 34.82% 83

154 0 "ITTCWTTTTT 11 ‘"11"r' ' ■ r ■" i111 r i" " i" " i" " r ■" r " ■ i" " i" " r " ■ i" " r "' i" " i mlz-> 40 60 80 100120140160180200220240260 280300320340360380400420 Abundance #93917: 2-cyanomethylene-3-oxo-1,2,3,4-tetrahydroquinoxaline 185 33.00 33.20 33.40 33.60 33.80

.. k m/z 112.10 29.72%

5000 157

90 । 131 0 " r " 'i' - r "11" " i" " i" " i" " i" " r "' i" " i" " r ■" i'"11" " i" " i1'" i miz-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 33 00 33.20 33.40 33.60 33.80

00463.D SCAN508.M Mon Jan 14 10:46:57 2002 Page 12

NYC-WTC_000051437

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