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GCMS results for sample AE00468, Jan 18 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00468 with surrogate recovery data on January 18, 2002.

NYC-WTC_000051318–000051335

Folder label: “GCMS X 1/8/02 A 1/10/02

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Scanned page image, NYC-WTC_000051334
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN10\00468.D Vial : 5 Acq On 10 Jan 2002 6:07 pm Operator: ’ Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 11 Decanedioic acid, bis(2-eth... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 33.40 1.09 ug/L 515064 Perylene-dl2 34.42 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Decanedioic acid, bis(2-ethylhex... 426 C26H50O4 000122-62-3 59 d 2 dl-2-Ethylhexyl chloroformate $$... 192 C9H17C1O2 024468-13-1 436ov9 3 2-Nonanol, 5-ethyl- (CAS) $$ 5-E... 172 C11H240 000103-08-2 38 AACH 4 Propanedioic acid, hexyl-, dieth... 244 C13H24Q4 005398-10-7 25 7 Abundance Scan 2630 (33.400 min): 00468.D (-) m/z 185.10 100.00% 185

57 5000 112 83 -|~i-r-r-r-|-r-r

/z-> Abundance 01 14 T* L l Il 143 JI 166 I ll i > i | > . > . | i f > i | Ti i

40 60 80 100120140160180200220240260280300320340360380400420 203 297 ' i ' " ' i" " i" "i ‘"11" "'r "1 r'" i" ■ ■ i " " i" " i 33.00 33.20 33.40 33.60 33.80 m/ Z 57.10 59.39% #345444: Decanedioic acid, bis(2-ethylhexyl) ester (CAS) $... 185 57 112 5000 I ' r ' • I ’ ' 33.00 33.20 33.40 33.60 33.80 m/z 71.10 41.25% 426 o1 i" ’11"' 11 ■ ‘ " r1 1IPI00"0‘0—010m210000900000—000300puam—0TT7 n/z-> 40 60 80 100120140160180200220240260280300320340360380 400420 Abundance #102311: dl-2-Ethylhexyl chloroformate $$ 2-Ethylhexyl chi... F7 112 11 | ‘ « 33 00 33.20 33.40 33.60 33.80 5000 83 m/z 70.10 39.35%

0 p| TYp-r 148 192 \ '■ r'" i'1" i" " r'1' i" " i"111111 ‘ 11"' r "' r " ■ r'" i" " i" " i" " i" " r'" i m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #76872: 2-Nonanol, 5-ethyl- (CAS) $$ 5-Ethyl-2-nonanol $$ ... ................ ................. 57 33 00 33.20 33.40 33,60 33.80 m/z 112.10 33.78% 5000 83 112

0 " i" ,Ti'"' iT'1 j " 154 >।■■•■। • i' i" • ■ । । । । ।। b *111 ‘111" ■' । । • 1 •" ■ 1 n/z-> 40 60 80 100120140160180200220240260280300320340360380400420 33.00 33.20 33.40 33.60 33.80

00468.D SCAN508.M Fri Jan 11 10:08:44 2002 Page 13

NYC-WTC_000051334

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NYC-WTC_000051334Source: NYC Law Department, mirrored locally

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