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GCMS results for sample AE00702, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00702 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000051895–000051913

Folder label: “GCMS X 1/10/02 A 1/16/02

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NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\5973N\02JAN16\00702.D Vial: 2 • Acq On : 16 Jan 2002 3 :57 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 11 Decanedioic acid, bis(2-eth... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 33.41 8.27 ug/L 4468420 Perylene-dl2 34.42 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Decanedioic acid, bis(2-ethylhex... 426 C26H50O4 000122-62-3 94 2 Decanedioic acid, bis(2-ethylhex... 426 C26H50O4 000122-62-3 72 3 Decanedioic acid, bis(2-ethylhex... 426 C26H50O4 000122-62-3 47 4 1-[4-[3-(2-chloro-9H-thioxahthen. .. 442 C24H27C1N2O2S 000000-00-0 47 Abundance Scan 2631 (33.412 min): 00702.D (-) m/z 185.10 100.00% 185

57 5000 112 I 83 TPTT

/z-> 0 28.1,4,41/4,17.343466 143 166 203 r1" 1' " ■ 1 268 297315 i" "i •1,1111 "'1" 40 60 80 100120140160180200220240260280300320340360380400420 r1111" " 1" " r'" r1" 1" " i 33 00 33.20 33.40 33.60 33.80 m/z 57.10 51.60% Abundance #345442: Decanedioic acid, bis(2-ethylhexyl) ester (CAS) $... 185

5000 57 112 3300 33,20 33.40 33.60 33.80 83 m/z 71.10 36.29% 143 166 203 298316 miz-> 0 ' " i"' v Hlamm 40 60 80 100120140160180200220240260280300320340360380400420 I' 1" " 1" " 1" " 1'1" I

Abundance #345443: Decanedioic acid, bis(2-ethylhexyl) ester $$ Seba. .. 185 i 1 ■ ■ ■ । 3300 33.20 33.40 33.60 33.80 5000 112 m/z 70.10 35.63% 71

297315 143 166 203 0 ............ - " ■ i" " i" " i" ‘ ■ 268 l l i'1" 11"f i"'11 ■"' i 408426 1" " r ‘" 1" " 1 "I Wz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #345444: Decanedioic acid, bis(2-ethylhexyi) ester (CAS) $... l ‘ ' I | ' 1 | ' ' ' 1 | i 165 33.00 33.20 33.40 33.60 33.80 57 m/z 112.10 :32.46%

.y 112 5000

0 426 I'" T’I"TTTI)ITI’“TTTTETTT*)UTTTTTTT’T ■ ' i Ui m/z-> 40 60 80 100120140160180200220 240260280 300 320 340360 380 400 420 33.00 33.20 33.40 33.60 33.80

)0702 .D SCAN508 .M Thu Jan 17 08:17:24 2002 Page 13

NYC-WTC_000051911

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NYC-WTC_000051911Source: NYC Law Department, mirrored locally

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