GCMS results for sample AE00702, Jan 29 2002

NYC 9/11 Public Portal Document

UaLY DCaLU wpOul ACPOLU

Data File : C:\MSDCHEM\1\5973N\O2JAN16\00702.D Vial: 2 • Acq On : 16 Jan 2002 3:57 pm Operator: Sample : 508scan Inst : Instrumen Mise 2002: January 16, Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 12 Octadecane (CAS) $$ n-Octad... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 34.12 0.21 ug/L 116079 Perylene-dl2 34.42 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane (CAS) $$ n-Octadecane... 254 C18H38 000593-45-3 72 2 Pentacosane $$ n-Pentacosane 352 C25H52 000629-99-2 64 3 Tridecane (CAS) $$ n-Tridecane $... 184 C13H28 000629-50-5 59 4 Nonacosane 408 C29H60 000630-03-5 59 Abundance Scan 2693 (34.119 min): 00702.D (-) m/z 57.10 100.00% 57

85

5000

113 "i 42

n/z-> 0/ H +rr L '' I’ ' ' ' 1<’> t > ■ ‘ 1 t ' ' ■ ■ ! ' ''1 I ' ' ' । I।' ' । I ' 1 ‘ ‘1 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 TTTI’uwT 33.80 34.00 34.20 34.40 m/z 71.10 74.83% Abundance #193184: Octadecane (CAS) $$ n-Octadecane $$ Octadecan 43 71 5000 33.80 34.00 34.20 34.40 m/z 85.10 66.82% 99 0- —H ..................................................... . I ' ' 1 ' I ' 1 ' '1 1 ' ' ' 1 1 1 1 ’ I miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 540 Abundance #300501: Pentacosane $$ n-Pentacosane 57 AARMAAAALL 33.80 34.00 34.20 34.40 5000 85 m/z 43.10 57.68% * , 113

n/z-> 0........ 40 60 L 141 1169 196 '' i' ■'' i ■1 ■ ■ i ■' ■11 ■ ■ ■ ■ r ■ ■ ■ i ■ ■ ■ ■ । 80 100 120 140 160 180 200 220 240 260 280 300 320 340 281296 ■ i ■ ■ ■ ■ r ■ ■ ■ r ' " i ■ 352 TT

Abundance #93375: Tridecane (CAS) $$ n-Tridecane $$ Tridecane, n- 57 33.80 34.00 34.20 34.40 m/z 55.10 24.25% 5000

iz--> 0 33 ■ i "■ 40 11 " ' l 85

1′131141156184...................... •I ‘ ‘‘T‘7 •> । >> । . । ■ । । । । । । « । । i i i । । m i । । i i i 11 i ′ । । । 11 । 11 i । । । mi I’TFIF 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 t/33.80 34.00 34.20 34.40

0702.D SCAN508.M Thu Jan 17 08:17:24 2002 Page 14

NYC-WTC_000051912