GCMS surrogate recovery results for sample AE00278, Jan 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\O2JANO9\278.D Vial: 3 Acq On 9 Jan 2002 7:50 pm Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 7 Octadecane (CAS) $$ n-Octad... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 33.26 0.13 ug/L 104235 Perylene-dl2 34.42 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Octadecane (CAS) $$ n-Octadecane... 254 C18H38 000593-45-3 38 2 Nonadecane (CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 27 3 Decane, 2-methyl- (CAS) $$ 2-Met... 156 C11H24 006975-98-0 27 4 Octadecane 254 C18H38 000593-45-3 22 Abundance Scan 2618 (33.263 min): 278.D (-) m/z 57.10 100.00% 57

43 71 85 5000 97 111 208 276 PA A AAA w! .... ............ 33.00 33.20 33.40 33.60 0 .............. m/z 71.10 63.82% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #193189: Octadecane (CAS) $$ n-Octadecane $$ Octadecan 57 71

£ 5000 85 33.00 33.20 33.40 33.60 m/z 43.10 59.87% 99 113 127 254

n/z-> 0- —P *Tr .I.• ' I 1 ‘ I._____________ 1 ' I ' ' ‘ ' I ' ' ' ’ I ' ’ ’ ' I ' ' ' ' I ' ' ' ' I ' '■ 1 1 i 1 ■ ‘ ’ i 1 100 120 140 160 180 200 220 40 (60 80 240 260 280 Abundance #211484: Nonadecane (CAS) $$ n-Nonadecane 57 71 MlWMWYHy. MTN 33 00 33.20 33.40 33.60 85 m/z 85.10 59.29% 5000

97

n/z-> 0- ' ■ I ’ ’ ' 1 i 1 1 40 60 —lL II 111 80 i 100 127 141 155 ■ ni 241 ..I ' i ■ 1 1 ■ i ■ ' ' 1 i ' ' ' • i ■ ■ ' ' i • ' 240 260 280 268

Abundance 120 140 160 180 #56249: Decane, 2-methyl- (CAS) $$ 2-Methyldecane $$ 2-Met... 200 220 .....A AAAA ' ' I 1 ' ' ' I 57 33.00 33.20 33.40 33.60 71 rn/z 55.10 26.52%

5000 85

99 113 141

/z-> 0-P 40 । ■ I ■ । I > • J 60 80 100 r... I, 156 120 140 160 180 200 220 240 260 280 33.00 33.20 33.40 33.60

278.D SCAN508.M Thu Jan 10 11:51:45 2002 Page 9

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