GCMS data file header for sample AE00700, Jan 16 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN16\00700.D Vial: 5 Acq On : 16 Jan 2002 2:11 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Octacosane $$ n-Octacosane Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

34.12 0.21 ug/L 109984 Perylene-dl2 34.42

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octacosane $$ n-Octacosane 394 C28H58 000630-02-4 59 2 Nonadecane 268 C19H40 000629-92-5 53 3 Heptadecane 240 C17H36 000629-78-7 53 4 Tetratetracontane 619 C44H90 007098-22-8 53 Abundance Scan 2693 (34.119 min): 00700. D (-) m/z 57.10 100.00% 57

5000 85

■ ■ l 1 • f 11 ‘T I

n/z-> 0 a113 135 1 ■f ■ i11" i1 I''1'I 207 1) I " " I " " I " ' 1 1 1 1 11 I ' 1 ' 1 I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 I ' T’’I r 33.80 34.00 34.20 34.40 m/z 71.10 63.56% Abundance #329266: Octacosane $$ n-Octacosane 57

5000 85 33.80 34.00 34.20 3440 ' ' m/z85.0550.65%

N 113 .. 0- 1.1.3.1191 , 169 , 196 224 350 ’ ’’’’’ TT711 ri f i 1 TI"011—*_*unuuunuOanut 394 TTsp 281 i1" ■ i /z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #211481: Nonadecane 57 W 33.80 34.00 34'20 ‘34'40 ' 5000 m/z 43.10 41.46%

N 85

iz-> 0 m I 1113141 169 ---------- T| ! I I 224 268 I | ITTTpi I I | ( I I I | I I " '' I'''111'r' I' ’ ’1’ 1 " I' 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #174551: Heptadecane 57 T 33.80 34.00 34.20 34.40 m/z 55.10 25.27% 5000 85 MWMWW/Aw | | J 113,141 169 210 240 o ।. i" > 111 > »i 11 r 111. j > f i > 1 ’*ti (T 111 > >i 1111111111111 > ' i" " i " " r Tl/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 33.80 34.00 34.20 34.40

)0700.D SCAN508.M Thu Jan 17 08:17:11 2002 Page 9

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