GCMS analysis results for sample AE01141, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB25\01141.D Vial: 7 Acq On : 25 Feb 2002 4:11 pm Operator: ■ Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Eicosane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

21.33 0.15 ug/L 106215 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 90 2 Octadecane (CAS) $$ n-Octadecane... 254 C18H38 000593-45-3 90 3 Nonadecane $$ n-Nonadecane 268 C19H40 000629-92-5 87 4 Hexadecane (CAS) $$ n-Hexadecane... 226 C16H34 000544-76-3 86 Abundance Scan 1591 (21.334 min): 01141 .D (-) m/ z 57.10 100.00% 57

71 fl 43 5000 85 P 99 21.00 21.20 21.40 21.60

m/z-> 0- 40 l 60 1 113 127 III nl i '1 1 * r । । । . . 100 120 ■ ' i ■ ' ■ ■ i ■ 1 140 160 180 200 220 240 260 280 m/z 71.10 63.44%

Abundance #228992: Eicosane 43 57 71 5000 N................................................... 85 21.00 21.20 21.40 21.60 m/ z 43.10 56.71% 99 113 127 141 282 0- J TBn n ’ 1 1 1 1 111 1 1 T1 111111G IT nlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #193184: Octadecane (CAS) $$ n-Octadecane $$ Octadecan 43 57 71 , AAAAAA-A--YMA W 21.00 21.20 21.40 21.60 5000 85 m/ Z 85.10 39.99%

QQ 11213127 141..................... 254....... n/z-> Abundance 0■ ' I 1 40 60

57 80 100 120 140 160 #211486: Nonadecane $$ n-Nonadecane 180 200 220 240 260 280 ’ I’’ 21.00 21.20 21.40 21.60 A.... 43 71 m/z 41.10 29.01% 85 5000

0■ ■ । ■ I 99Il , .. I I ML 1 ' ' 113.127 .............. 183 197 .... .............. 266 M- ------------ m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 21.00 21.20 21.40 21.60

01141.D HP022102.M Tue Feb 26 08:30:26 2002 Page 10

NYC-WTC_000003556