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GCMS analysis results for sample AE01141, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01141 conducted on February 27, 2002.

NYC-WTC_000003543–000003562

Folder label: “GCMS X 1/20/02 A 2/25/02”

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Scanned page image, NYC-WTC_000003557
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02FEB25\01141.D Vial : 7 Acq On : 25 Feb 2002 4:11 pm Operator: . • Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 9 Undecane, 3,6-dimethyl- Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 21.40 0.06 ug/L 38789 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Undecane, 3,6-dimethyl- 184 C13H28 017301-28-9 64 2 Octane, 3,6-dimethyl- 142 C10H22 015869-94-0 45 3 Decane, 2,6,8-trimethyl- 184 C13H28 062108-26-3 42 4 Undecane, 6,6-dimethyl- 184 C13H28 017312-76-4 40 Abundance Scan 1597 (21.402 min): 01141 .D (-) m/z 57.10 100.00% 57 71

43 5000

0 11111 ■ r ■ ■' i' — rp-r 85 99

P—TP1PmIPWPRTTTTTTTT 113 . W. 21.00 21.20 21.40 21.60 21.80 m/ z 71.10 94.47% mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #93412: Undecane, 3,6-dimethyl- 57

5000 A I 71 21.00 21.20 21.40 21.60 21.80 m/z 43.10 53.61%

niz-> O—PPPTT + 2598.113.... 155... 184 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #38860: Octane, 3,6-dimethyl- 57 71 AAAA--A-AAA 21.00 21.20 21.40 21.60 21.80 5000 m/z 41.10 42.88% 113 85 0- ■ i * ■27 42 142 ■ ■ i • ■ ■ > 11 * ■ • । ■ 4m ------- ' i " ■' i1" ' i " " i " " i " " r ■ ■11'

miz- > 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #93449: Decane, 2,6,8-trimethyl- M... 1 i ■ ■ ■ ■ i ■ ■ 57 21.00 21.20 21.40 21.60 21.80 m/z 56.00 32.30%

5000 43 71

n/z—> O-PPO ml .. .... 113 85 99 119 155 184 ■ i ■ ■1■i'■•11 ■ ■111 ■ ■ ■•i■ ■'1111 ’11 ■■■■i■ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ....... ' 1 1 1 1 1 1 1 1 1 21.00 21.20 21.40 21.60 21.80

01141.D HP022102.M Tue Feb 26 08:30:26 2002 Page 11

NYC-WTC_000003557

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NYC-WTC_000003557Source: NYC Law Department, mirrored locally

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