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GCMS analysis results, Feb 27 2002

Machine-extracted title · confidence 90%

Gas chromatography-mass spectrometry results for sample AE01138 identifying unknown compounds and surrogates on February 27, 2002.

NYC-WTC_000003463–000003482

Folder label: “GCMS X 1/20/02 A 2/25/02

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Scanned page image, NYC-WTC_000003481
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB25\01138.D Vial: 4 . Acq' On : 25 Feb 2002 1:43 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 13 O-DIMETHYLAMINOBENZALDEHYDE... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

24.85 0.07 ug/L 41793 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 O-DIMETHYLAMINOBENZALDEHYDE $$ B... 149 C9H11NO 000579-72-6 78 2 1,2-Benzenedicarboxylic acid, bu... 278 C16H2204 017851-53-5 64 3 Dibutyl phthalate $$ 1,2-Benzene... 278 C16H2204 000084-74-2 64 4 diisobutyl benzene-1,2-dicarboxy... 278 C16H2204 000000-00-0 9 Abundance Scan 1902 (24.845 min): 01138.D (-) m/z 149.00 100.00% 149

5000

41 57 93 . 223 24.60 24.80 25.00 25.20 0J , I, ., 1.......1.7........ . , . , , । , I . ....... . ,।, 1 m/z 149.90 10.06% Tl/Z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #45220: O-DIMETHYLAMINOBENZALDEHYDE $$ Benzaldehyde, 2-(di... 149

44 120 77 106 5000 132 IIIII11* 1 1 I ’ 1 1 ■ l ■ ■ 91 24.60 24.80 25.00 25.20 m/z 41.10 9.47%

0—7 m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223230:1,2-Benzenedicarboxylic acid, butyl 2-methylpropy... 149

24.60 24.80 25.00 25.20 5000 m/ z 57.00 7.08%

97 41 57 76 104 121 205 223 278 0 - TPO—_gT m/z-> :20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223242: Dibutyl phthalate $$ 1,2-Benzenedicarboxylic acid... 149 24.60 24.80 25.00 25.20 m/z 223.00 6.89%

5000

41 56 76 104 121 205 223 278 0--------- I I

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 24.60 24.80 25.00 25.20

01138.D HP022102.M Tue Feb 26 08:30:04 2002 Page 15

NYC-WTC_000003481

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NYC-WTC_000003481Source: NYC Law Department, mirrored locally

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