GCMS analysis results for sample AE01142, Feb 2002

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Laboratory report documenting GCMS analysis of sample AE01142 conducted on February 27, 2002.

NYC-WTC_000003523–000003542

Folder label: “GCMS X 1/20/02 A 2/25/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB25\01142.D Vial: 8 Acq On : 25 Feb 2002 5:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 1,2-Benzenedicarboxylic aci... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 24.85 0.12 ug/L 79361 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, bi... 282 C14H1806 000117-82-8 83 2 Dibutyl phthalate 278 C16H2204 000084-74-2 83 3 Dibutyl phthalate 278 C16H2204 000084-74-2 83 4 1,2-Benzenedicarboxylic acid, bu... 334 C20H30O4 000085-69-8 83 Abundance Scan 1902 (24.845 min): 01142.D (-) m/z 149.00 100.00% 149

5000

41 57 76 93 24.60 24.80 25.00 25.20 1 205 223 m/z 150.00 7.82% 0 ■ 1,4 ’i ' ~i ' ' r । * । ‘I ' ■' < I’ ' * ' I ' 1 1 1 1 1 1 1 ' I ' 1 1 ' I ' ' lz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #227809:1,2-Benzenedicarboxylic acid, bis(2-methoxyethyl)... 149 ................. |.......................

5000 24.60 24.80 25.00 25.20 m/ z 41.10 6.97% 41 56 76 104 121 N 205 223 282 0-■ 1 i ' IP m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223236: Dibutyl phthalate 149 IIIITT’II ■ ■ i ■ 1 1 r i ■ ■ 24.60 24.80 25.00 25.20 5000 m/z 223.10 5.24%

57 76 93 105 121 205 223 278 0- ■ i ■ ■ 1 ■'1 TPPp 1 I ' 1 1 1 1 1 11 I I .' । । ( I 1 I > I .... I I I I । । I | rr -il । > > ■ I । । m/z- > 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223237: Dibutyl phthalate 149 24.60 24.80 25.00 25.20 m/ z 57.10 5.07%

5000

41 56 76 104 121 205 223 278 0 ' ■ i ' 111. . I' । . . .'. | r . . . "i . I I | . i । i . । . । i । । i । r i . । ।. i i । । । . . । । . । । । . । 1 ' 1 1 1k 1 1 . . i . . . . । * . n/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 24.60 24.80 25.00 25.20

31142.D HP022102.M Tue Feb 26 08:30:35 2002 Page 14

NYC-WTC_000003540

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