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GCMS analysis results for sample AE01141, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01141 conducted on February 27, 2002.

NYC-WTC_000003543–000003562

Folder label: “GCMS X 1/20/02 A 2/25/02”

←Page 18 of 20→
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02FEB25\01141 .D Vial: 7 Acq On : 25 Feb 2002 4:11 pm Operator: • Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ******************************************************************** * Peak Number 12 Phthalic acid, butyl ester, ... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

24.84 0.09 ug/L 66372 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phthalic acid, butyl ester, este... 336 C18H24O6 000085-70-1 83 2 Dibutyl phthalate 278 C16H2204 000084-74-2 83 3 Dibutyl phthalate $$ 1,2-Benzene... 278 C16H2204 000084-74-2 83 4 1,2-Benzenedicarboxylic acid, di... 278 C16H2204 000084-74-2 83 Abundance Scan 1902 (24.845 min): 01141. D (-) m/z 149.00 100.00% 149

5000

41 57 — 76 104 | 205 223 24.60 24.80 25.00 25.20 0- ___________ |___________________ L____ ]_______________ ' 1 1 ‘ ' 1 I ' 1 ' ' 1 1 ‘ 1 1 1 1 ' ' 1 1 ‘ 1 ' ' 1 ‘ 1 1 1 1 1 1 ' 1 1 ' 1 m/Z 150.00 12.53% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #286375: Phthalic acid, butyl ester, ester with butyl glyc... 149

5000 24.60 24.80 25.00 25.20 m/ z 41.10 9.22% 57 76 104 121 167 205 223 278 04 1 I ' 1 1 I H ? i । I11 । । M PT ■ i ■ ■ ■ ■ ■ i ■ > ■ ■। ■

/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223233: Dibutyl phthalate 149

24.60 24.80 25.00 25.20 5000 m/z 57.10 6.53%

57 76 104 121 205 223 278 250 01----- TTT ■ i 1 ‘ ‘I ■ ■ . । > < . । । . . . । । .- ■ । ■ i • ■ ■ ■ । ■ । miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223242: Dibutyl phthalate $$ 1,2-Benzenedicarboxylicacid... 1 1 i ' 1 1 1 1 ' ' 1 i 1 1 1 1 i ■ ' 149 24.60 24.80 25.00 25.20 m/ z 104.00 5.72%

5000

41 56 76 104 121 205 223 278 01 ■ I i ■ ■■i'l'| ■ I'| । | I'■ ■ ■ 7'| ■ । ■ I rr. . । , rT , । r mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 24.60 24.80 25.00 25.20

01141.D HP022102.M Tue Feb 26 08:30:27 2002 Page 14

NYC-WTC_000003560

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NYC-WTC_000003560Source: NYC Law Department, mirrored locally

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