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GCMS analysis results for sample AE00169, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.

NYC-WTC_000050519–000050538

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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Scanned page image, NYC-WTC_000050537
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LJJLaLy OCaLti ~opoul RCpUa

Dats File : C:\MSDCHEM\1\5973N\02JAN24\00169.D Vial: 2 ‘ Acq On : 24 Jan 2002 3:48 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 Dibutyl phthalate Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

24.85 0.07 ug/L 53153 Phenanthrene-dl0 22.65

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Dibutyl phthalate 278 C16H2204 000084-74-2 83 2 Dibutyl phthalate 278 C16H2204 000084-74-2 83 3 1,2-Benzenedicarboxylic acid, di... 278 C16H2204 000084-74-2 83 4 1,2-Benzenedicarboxylic acid, bu... 278 C16H2204 017851-53-5 83 Abundance Scan 1881 (24.849 min): 00169.D (-) m/z 149.00 100.00% 149

5000

41 56 76 1.....}........... I... i1 ■ 104 121 , 205 223 m/z ... a... 24.60 24.80 25.00 25.20 41.10 9.87% m/z-s 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223233: Dibutyl phthalate 149

5000 ’ • | ‘ | 1 • i ■ ■ ■ ■ i ■ ■ 24.60 24.80 25.00 25.20 m/z 150.00 8.26% 76 57 104 121 205 223 250 278 niz-> ommapondly 20 40 60 — loshuosdyfesi P 80 100 ।। 120 140 160 180 200 220 240 260 280 ।.—— ■ I 1 ■ 11 I ■ • ■ • i' ■ Abundance #223232: Dibutyl phthalate 149 ■ ' i • > । * T 24.60 24.80 25.00 25.20 5000 m/z56.10 6.11%

29 41 57 76 104 121 163 178 295 223 IdaIpauapeaFfagBui - f m i' . r'' ■. i ■■' ■' p ' " i' " ■ i " " rr r m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223238:1,2-Benzenedicarboxylic acid, dibutyl ester (CAS)... 149 24.60 24.80 25.00 25.20 m/z57.00 5.64%

5000

57 76 104 205 223 -- 121 188 278 • i.■ • -1 • • * - I * • miz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 24.60 24.80 25.00 25.20

00169.D SCAN508.M Fri Jan 25 10:26:00 2002 Page 15

NYC-WTC_000050537

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NYC-WTC_000050537Source: NYC Law Department, mirrored locally

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