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GCMS analysis results for sample AE00562, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis results for sample AE00562 conducted on February 1, 2002.

NYC-WTC_000051567–000051585

Folder label: “GCMS X 1/9/02 A 1/29/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN29\00562.D Vial: 4 Acq On : 29 Jan 2002 1:02 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************** * * ******** * Peak Number 12 Dibutyl phthalate Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

24.85 0.12 ug/L 94439 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm . CAS# Qual

1 Dibutyl phthalate 278 C16H2204 000084-74-2 83 2 1,2-Benzenedicarboxylic acid, bu... 278 C16H2204 017851-53-5 83 3 1,2-Benzenedicarboxylic acid, bi... 278 C16H2204 000084-69-5 78 4 Dibutyl phthalate 278 C16H2204 000084-74-2 78 Abundance Scan 1881 (24.849 min): 00562. D (-) m/z 149.00 100.00% 149

5000

41 56 76 104 121 | 24.60 24.80 25.00 25.20 0. - 205 223 m/z 150.00 9.72% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223233: Dibutyl phthalate 149

5000, 1 11 1 1 ' 1 i'' 11 f ' FT 24,60 24.80 25.00 25.20 m/ z 41.10 7.48% 57 205 223 i 111 11 11 1 I11''r 76 104 121 ' 1 • ‘ 1 ' 1 1 ' ' 1 250 278 —— ' i 1 ■ 1 ' i ■ ■ 1 1 i 1 /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223230:1,2-Benzenedicarboxylic acid, butyl 2-methylpropy... 149 T’TuummTTTTTr 2460 24.80 25.00 25.20 5000 m/z 56.10 5.50%

27 41 57 76 104 121 1 205 223 278 ........... .. । । । ■ t • f1 1 ■ ■ l ■ ■ i ■ n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223249:1,2-Benzenedicarboxylic acid, bis(2-methylpropyl)... ItI" 1TTT ' ' I ' ' ' ' I ' ' 149 24.60 24.80 25.00 25.20 m/z 57.10 4.48%

5000

57 76 104 --PPP 121 45 । 163 205 223 236 278 1 T" 11 I 11 1 .... 1 ... . I l’. . OTT T-|-r-TT-r-p-r-r-r-p-r ■ ■ ।■ r /z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 24.60 24.80 25.00 25.20

00562.D SCAN508.M Wed Jan 30 09:02:04 2002 Page 14

NYC-WTC_000051584

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NYC-WTC_000051584Source: NYC Law Department, mirrored locally

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