GCMS analysis results for sample AE03075, March 5 2002

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Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.

NYC-WTC_000010927–000010946

Folder label: “GCMS X 2/5/02 A 2/28/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB28\02716 .D Vial: 1 Acq On : 28 Feb 2002 2:40 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 8, 2002 Multiplr: 1..00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 Dibutyl phthalate $$ 1,2-Be... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 24.86 0.08 ug/L 47657 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Dibutyl phthalate $$ 1,2-Benzene... 278 C16H2204 000084-74-2 83 2 Dibutyl phthalate 278 C16H2204 000084-74-2 83 3 1,2-Benzenedicarboxylic acid, bu... 278 C16H2204 017851-53-5 83 4 Dibutyl phthalate 278 C16H2204 000084-74-2 83 Abundance Scan 1903 (24.857 min): 02716.D (-) m/z 149.00 100.00% 149

5000-

T T T -j-r-T 41 . 205 223 24.60 24.80 25.00 25.20 — 56 76 104 0- -- •i•'■■i■11 ■ i ■ ■1 ■ 1 • ■ ■ 11 ■' ■ ■ 1 ■1‘‘11111111 r ■ 11 m/z 150.00 9.68% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223242: Dibutyl phthalate $$ 1,2-Benzenedicarboxylic acid... 149

5000 24.60 24.80 25.00 25.20 m/z 41.10 7.59% 41 56 76 104 121 205 223 278 0 “I " , , . । . r. . । . . . 1 । 1 1 1 1 । r n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223237: Dibutyl phthalate 149

24.60 24.80 25.00 25.20 5000 m/z 205.10 4.95%

41 0 .. I, 56 76 104 121 205 223 i *' * ■ i ' Af/ao/MamamampAoaguBe r> 1' i''11 ' i ■ 1 ■ • i ■ ■ ■ ■ i ■ 278 /z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223230:1,2-Benzenedicarboxylic acid, butyl 2-methylpropy... -r-r-j-r-n-r-p-r ■ ■ i ‘ ' i 149 24.60 24.80 25.00 25.20 m/z 223.10 4.83%

5000

27 41 57 76 104 121 205 223 278 0J - "IT’1’111111111111/1*111111111*T1*111*33315 11 mfa-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 24.60 24.80 25.00 25.20

02716.D HP022102.M Fri Mar 01 10:07:15 2002 Page 14

NYC-WTC_000010944

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NYC-WTC_000010944Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE03075, March 5 2002 · Box DEP Box 14

NYC-WTC_000010907

Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.

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