GCMS analysis report for sample AE01507, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02FEB21\01508.D Vial: 8 Acq On : 21 Feb 2002 9:01 pm Operator: Sample : 508 scan fb Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 Dibutyl phthalate Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 24.86 0.05 ug/L 38677 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dibutyl phthalate 278 C16H2204 000084-74-2 74 2 Dibutyl phthalate $$ 1,2-Benzene... 278 C16H2204 000084-74-2 74 3 Dibutyl phthalate 278 C16H2204 000084-74-2 64 4 Dibutyl phthalate 278 C16H2204 000084-74-2 64 Abundance Scan 1903 (24.857 min): 01508.D (-) m/z 149.00 100.00% 149

5000 ■ ■ i ■ ■ ■ ■ i ■ ■

41 57 76 105 223 24.60 24.80 25.00 25.20 nz—> 0 20 onaian)ya 40 — ■ i ■1 ■ ■ • i' * • 11 ■ ■ 1 ■ ■ i ■ ■ ‘ * i ■ ■ ■ • I ■1 ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ' i ■ ■ • • i ■ 60 80 100 120 140 160 180 200 220 240 260 280 m/z 150.10 9.38% Abundance #223232: Dibutyl phthalate 149

5000 1 ' i • ■ ■ 1 i ■ » > l * * * • l » । 24.60 24.80 25.00 25.20 m/z 41.10 9.06% 29 41 57 76 104 121 | 163 178 205 223 j 1 0 -----------t----1PPIP- miz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223242: Dibutyl phthalate $$ 1,2-Benzenedicarboxylic acid... 149 T T 18.8 24.60 24.80 25.00 25.20 5000 m/z 223.00 6.55%

41 56 76 104 121 205 223 278 0------ ■ 1 ■ > * i * ■ • । ।11 ।..j।, n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #223244: Dibutyl phthalate 149 24.60 24.80 25.00 25.20 m/z 57.00 6.22% 5000

57 76 104 121 205 223 274 01.... ।. +44 7. 11', ■ • P | | | 'l . . | m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 24.60 24.80 25.00 25.20

01508.D HP022102.M Mon Feb 25 10:54:58 2002 Page 14

NYC-WTC_000010003