GCMS analysis report for sample AE01507, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB21\01508 .D Vial: 8 Acq On : 21 Feb 2002 9:01 pm Operator: Sample : 508 scan fb Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 1,2-Benzenedicarboxylic aci... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 31.10 0.05 ug/L 33793 Chrysene-dl2 30.49 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 000117-84-0 42 2 1,2-Benzenedicarboxylic acid, mo... 278 C16H2204 004376-20-9 36 3 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 027554-26-3 9 4 1,10-Decane-l, 1,10,10-d4-diol (CAS) 178 C10H18D4O2: 067986-07-6 9 Abundance Scan 2456 (31.099 min): 01508.D (-) m/z 149.00 100.00% 149

5000 57 167 83 120 30.80 31.00 31.20 31.40 O' ’ 1—20923-111777177 ’’01——9—B09uuuEuuuT m/z 167.00 36.83% mfz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #326898: 1,2-Benzenedicarboxylic acid, dioctyl ester (CAS)... 149

5000 ■ ■ i 1 ■ ■ ‘ i ■ 1 ' I 1 ' ' ‘ I' ' 57 167 30.80 31.00 31.20 31.40 m/z 57.10 32.61% 390 I —mmmummaununnm 0-TI—muI —nuu niz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #223274:1,2-Benzenedicarboxylic acid, mono(2-ethylhexyl)... 149

30.80 31.00 31.20 31.40 5000 m/z 70.00 25.55% 70 167 112 0- 42 HHHmm K 93 ।1 “ ■ ।1 ■ ■ ■ । • • ■ ■ i “ ■■।■■।■■ ■ • i ■ ■1 ■ । “ ■ ■ । n/z—> 40 60 80 1(X) 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #326922:1,2-Benzenedicarboxylic acid, diisooctyl ester (C... ‘ 1 I ‘ 1 ■ ■ l ‘ ' I ‘ ‘ • I ‘ ‘ 149 30.60 31.00 31.20 31.40 m/z 55.10 21.23% 5000 57 167

1.............. 0 . 11.... ’* . । ।।। .............................................390 H .... j.. 11111 ri] 11111 n ■ ■ 111111111111, IT017 111 ■ 11111 u 11111 * ■ i ■ ■ ■ ‘ i ■ ' i ■ • ■ ■ i • ‘ miz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 30.80 31.00 31.20 31.40

01508.D HP022102.M Mon Feb 25 10:54:58 2002 Page 15

NYC-WTC_000010004