GCMS analysis report for sample AE01547, March 2002

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GCMS laboratory results for sample AE01547 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010066–000010085

Folder label: “GCMS X 1/23/02 A 2/21/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB21\01547.D Vial: 3 Acq On : 21 Feb 2002 4:52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 1,2-Benzenedicarboxylic aci... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 31.10 0.04 ug/L 25436 Chrysene-dl2 30.49 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, bi... 390 C24H3804 000117-81-7 78 2 (IS*,2R*,5R*,7S*)-2,4-Dimethyl-7... 168C10H16O2 091926-28-2 64 3 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 027554-26-3 59 4 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 027554-26-3 56 Abundance Scan 2456 (31.099 min): 01547.D (-) m/z 149.00 100.00% 149

5000 57 167 84 113 T 30,80 31.00 31.20 31.40 0 |_।।.... ।. >.. ।236 . 111 m/z 167.00 32.20% ' I"'111 ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #326907:1,2-Benzenedicarboxylic acid, bis(2-ethylhexyl) e... 149

5000 ■ ' i ■ 1 ■ ' i ■ ■ ■ i ' ■ ■ ■ i ■ ■ 57 167 30.80 31.00 31.20 31.40 m/z 57.10 32.16% 1 83 113 0- mH ' | ‘ !'' ■ ■ | ‘ |■ ■ ■ ■ | > 11 “ ' I ' " ‘ I " " I ‘ ' I ‘“ I “ " I “ ' । I ' 1 ' ‘ I

niz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #70509: (1 S*,2R*,5R‘,7S*)-2,4-Dimethyl-7-ethyl-6,8-dioxabi... 149 • • i > • > < i • ■ i ' ■ ■ ■ i ■ ‘ 30,80 31.00 31.20 31.40 5000 167 m/z 43.10 31.72% 71 113 0 T’—000—0——0B———mB000307 ■ H1।111111।।।।।11.... j n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #326922:1,2-Benzenedicarboxylic acid, diisooctyl ester (C... 149 30,80 31.00 31.20 31.40 m/z 71.10 21.41% 5000 57 167

0' •H"" |" "I'‘"l'“‘l "“I' ___ ..।.... ।.... ।.... ।.... ।_____ ।.... ।390 .... ।.... ।.... ।.... ।.... ।.... _ .... । -r-r-j-r-r-n-j-r ■ ' I ' ' ' ■ I ■ ■ /z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 30.80 31.00 31.20 31.40

01547.D HP022102.M Mon Feb 25 10:55:26 2002 Page 15

NYC-WTC_000010084

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GCMS analysis report for sample AE01511, March 2002 · Box DEP Box 14

NYC-WTC_000010047

GCMS laboratory results for sample AE01511 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

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