GCMS analysis report for sample AE01547, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB21\01547 .D Vial: 3 * Acq On : 21 Feb 2002 4:52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 2-Ethylformanilide Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

24.86 0.03 ug/L 20715 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Ethylformanilide 149 C9H11NO 002860-30-2 2 2 Furo[2,3-c]pyridine, 2,3-dihydro... 149 C9H11NO 069022-82-8 2 3 5-Methyl-7-amino-S-triazolo(1,5-... 149 C6H7N5 033376-96-4 2 4 Benzenebutanamine (CAS) $$ 4-Phe... 149 C10H15N 013214-66-9 1 Abundance Scan 1903 (24.857 min): 01547.D (-) m/z 149.00 100.00% 1-9

5000

41 24.60 24.80 25.00 25.20 0- .49 m/z41.10 12.97% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #45251:2-Ethylformanilide 1-9

106 120 5000 ' ' I ' i 1 ' 24.60 24.80 25.00 25.20 132 77 91 m/z 44.00 0.63%

miz-> 0- ■ ■ i 1 1 1 • i • ■ ■ ■ i ■ ■ 1 ' i ■ ■ ■' i ■ ■ ■ ■ I ‘ ■ ■ ■ i ‘ ' 40 50 60 70 80 90 100 110 120 130 140 ... • ■ j - • ■ • i ■ > 150 wAwwyNWWN Abundance #45246: Furo[2,3-c]pyridine, 2,3-dihydro-2,7-dimethyl- $$... 1-9

120 24.60 24.80 25.00 25.20 5000 m/z 48.95 0.28% 79 134 106 51 65 93 NMA Ai A J N

miz-> 0 — 40 L 50 ... . t, ,, t — 60 70 80 90 100 110 120 130 140 150 ’ I* Abundance #44981:5-Methyl-7-amino-S-triazolo(1,5-A)pyrimidine $$ (1 ... ’i • ■ ‘ i ■ 1 ■ ' i 1-9 24.60 24.80 25.00 25.20

5000

109 122

mfe-> 0 .40........... 70 81... 91 • 1 I 1 ■ ' ‘ i 1 ■ ' ' i ■ ■ ■ ■ i • ■ ■ ■ i ' ■ ■ ■ i ■ • ‘ ■ i ' ■ ■ 1 i ■ ■ ' II 50 60 80 90 100 110 134 *’I’’*I**’I’* 120 130 140 150

01547.D HP022102.M Mon Feb 25 10:55:26 2002 Page 14

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