GCMS blank results for sample AE03509, March 28, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03509.D Vial: 5 Acq On : 8 Mar 2002 1:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 2-Furanmethanol, tetrahydro... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

5.71 0.11 ug/L 55983 1,4-Dichlorobenzene -d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual/ 1 2-Furanmethanol, tetrahydro- (CA... 102 C5H10O2 000097-99-4 42 2 3-Buten-2-ol, 3-methyl- (CAS) $$... 86 C5H10O 010473-14-0/12 3 Thioformyl cyanide 71 C2HNS 000000-00-0 9 4 3-Buten-2-ol, 2-methyl-______________ 86 C5H10O 000115-18-4 9 Abundance Scan 207 (5.711 min): 03509. D (-) m/z 41.10 100.00% 41 71 —

5000 45 - — — 53 58 84 5.40 5.60 5.80 6.00 — O+ +4 m/z 43.10 88.41% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #9384: 2-Furanmethanol, tetrahydro- (CAS) $$ Tetrahydrofur... 7(1 43

5000 27 — — -P - 31 5.40 5.60 5.80 6.00 m/z 71.00 82.30% 53

miz—> 0 • • i ■ • • • i ■ TTIT - — 37 4+ MA1 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 ।11111■'।।■ ■ ■ ■ । । ■ 95 Abundance #4092: 3-Buten-2-ol, 3-methyl- (CAS) $$ 3-METHYL-3-BUTEN-2... 43 -A 5.40 5.60 5.80 6.00 ‘ ‘ 1 7 1 ‘ ‘ I

5000 39 m/z 69.00 48.07%

53 58 86 67 71 Of IUUUI-E—UIII—II0-T T - ■!■■■' 11-■ ’I- ■ i" ■ ■ i ‘ miz—> 60 65 70 75 80 85 90 95 Abundance 20 25 30 35 40 45 50 55 #1427: Thioformyl cyanide -4 41 71 5.40 5.60 5.80 6.00 m/z 45.00 33.21% 45 5000

01 ■ ■ i ■ • ■ ■ i'''111'1 ■ I ‘1 T ‘ ‘ I “ " I' ‘‘ I ‘ ‘ ‘ ' I' ' TII—I0DBTITTTT T-iqp-T-r-r-r-r-TT-i 1117TIn—II miz-> 20 25 30 35 404550556065 70 75 80 85 90 95 5.40 5.60 5.80 6.00

03509.D HP022102.M Fri Mar 15 10:08:58 2002 Page 9

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