GCMS blank results for sample AE03509, March 28, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report * Data File : C: \MSDCHEM\1\5973N\02MAR08\03509.D Vial: 5 Acq On : 8 Mar 2002 1:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 3-Buten-2-ol, 2-methyl- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 5.01 0.22 ug/L 111098 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 80 2 Butenol, methyl- 86 C5H10O 060766-00-9 59 3 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 59 4 1-Hydroxy-2-pentanone $$ 2-Penta... 102 C5H10O2 064502-89-2 53 Abundance Scan 145 (5.011 min): 03509. D (-) m/z 71.10 100.00%l 43 71

5000 55 P vy X A. I...... I ' ' TTPT ‘ I ‘ ‘ ' I ' ■ ' ' I ' ' 4.60 4.80 5.00 5.20 5.40 | O-pmpp m/z 43.10 96.55% mlz~> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #4085:3-Buten-2-ol, 2-methyl- 43 71

5000 A1 4 45 A A 59 4.60 4.80 5.00 5.20 5.40 27 m/z 41.10 69.61?

mz-> 44 0 ..।.... ।.... ।.... । m. । 86 hpmpmppp]ppm 10 2030405060 70 8090100110120130140150160170180190200210 Abundance #4093: Butenol. methyl- 43 71 LAAry , Aw \ A A , A . 4.60 4.80 5.00 5.20 5.40 5000 59 m/z 69.10 42.14! 27 15

miz-> 0- mlut I, ! 86 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #4084: 3-Buten-2-ol, 2-methyl- A....... A,............. . . , 43 71 4,60 4.80 5.00 5.20 5.40 m/z 55.00 34.57 5000

N 59

m/z—> 27 , । hill 0 "’—IE1ET010131111 '' ‘ I “Il'1L.1'' "I 861 ________________________________________ ... 1. .-1.1.... 1.... I <... 1||(||. AAL 1 -A 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 4.60 4.80 5.00 5.20 5.40

03509.D HP022102.M Fri Mar 15 10:08:58 2002 Page 8

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