Laboratory report documenting GCMS analysis of a method blank for sample AE03614 to verify analytical system cleanliness.
NYC-WTC_000037740–000037759Folder label: “GCMS X 2/19/02 A 3/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report * Data File : C:\MSDCHEM\1\5973N\02MAR08\03614.D Vial: 4 Acq On : 8 Mar 2002 6:03 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 3-Buten-2-ol, 2-methyl- Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T. 5.02 0.11 ug/L 51413 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 2 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 64 3 Hydroxylamine, 0-(3-methylbutyl)... 103 C5H13NO 019411-65-5 53 4 3-hydroxy-4,4-dimethyl .gamma. B... 130 C6H10O3 052126 0-6 50 Abundance Scan 146 (5.022 min): 03514.D (-) m/z 71.00° 100.00% 43 71
5000 59 AA_ —IaBT 1 1 ' | i i 53 4.60 4.80 5.00 5.20 5.40 04 TIT‘‘211‘1771‘‘‘1 TOTTH I 1 mHTTTRT 86 m/z 43.00 97.69% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #4085: 3-Buten-2-ol, 2-methyl- 7h 43
5000 59 LAAAAADA 4,60 4.80 5.00 5.20 5.40 27 m/z 41.10 63.32% Of ■ ■ i “ “ i‘ ’ 1 ■' i ■' “ i “ HH 86 miz—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110
ANuha Abundance #4084:3-Buten-2-ol, 2-methyl- 43 7 A 4.60 4.80 5.00 5.20 5.40 5000 m/z 69700 39.13% 59
27 53 86 miz-> 0 -mm yp-r tH tmmmmmm mp 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 Abundance #9886: Hydroxylamine, O-(3-methylbuty!)- $$ Hydroxylamine,... I 1 1 1 1T1 ' 1 1 1 T-T-pr r i ; p-n— 43 4.60 4.80 5.00 5.20 5.40 m/z 59.00 37.97% 5000 55 71
0 TI—TI TTnl—TgT H+ 103 I I » I I J i I I I I I 1 I I I 11 I I>1»I I»tI ItI I 11 I I I J I I > A......... _ i.........A 1 1 ‘ * 1 t ‘ ‘ ‘ 1 1 ‘ ’ i • ■ ■' । ■ miz—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 4.60 4.80 5.00 5.20 5.40
03514.D HP022102.M Fri Mar 15 10:09:23 2002 Page 9
NYC-WTC_000037752
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NYC-WTC_000037635
Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037760
Laboratory report documenting GCMS analysis of a method blank for sample AE03615 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037720
Laboratory report documenting GCMS analysis of a method blank for sample AE03612 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037780
Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037660
Laboratory report documenting GCMS analysis of a method blank for sample AE03509 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037800
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03617 conducted on March 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037680
Laboratory report documenting GCMS analysis of a method blank for sample AE03510 to verify analytical system cleanliness.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037700
Laboratory report documenting GCMS analysis of a method blank for sample AE03611 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009966
Analytical results for sample AE01508 analyzed via GCMS on March 4, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010106
GCMS laboratory results for sample AE01637 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010887
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · similarity 0.997
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Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.
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