GCMS analysis results for sample AE00248, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN24\00248.D Vial: 4 Acq On : 24 Jan 2002 5:27 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N .L ********************************************************************* Peak Number 6 3-Buten-2-ol, 2-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

5.02 0.29 ug/L 144960 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW. MolForm CAS# Qual

1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 78 2 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 72 3 Butenol, methyl- 86 C5H10O 060766-00-9 64 4 3-Buten-2-ol, 2-methyl- $$ .alph... 86 C5H10O 000115-18-4 56 Abundance Scan 144 (5.018 min): 00248. D (-) m/z 71.10 100.00% 43 71

5000 59 39 55 MM . N . 4.60 4.80 5.00 5.20 5.40

m/z—> TIPTPTT +74444 84w 67 I ■ ■ 11 ‘ ‘ 111 J | h ■ ■ | ■ i ■ i | 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 m/z 43.10 88.53% Abundance #4084:3-Buten-2-ol, 2-methyl- 71 43

5000 - —----A-4444 59 4.60 4.80 5.00 5.20 5.40 m/ z 41.10 57.32% 27 53 67 86 THHH —ppT '1 • ‘ I' ■' ‘ I' “' I'''' I'' ‘ ‘ I' “ • I' ‘ ‘' I'1 Tp-rr /z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #4083:3-Buten-2-ol, 2-methyl- 71 43 r 4N . A 4.60 4.80 5.00 5.20 NAf * ’ I ' ’ 4 5.40 5000 m/ z 59.10 39.34% 59 27 31

/z—> 5 1001aut1091—2——83T -37+ »• l • • • 11 ........ . 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 T

I 4 • 4 ‘ I ‘ M v A 4 Abundance #4093: Butenol, methyl- A 43 71 4.60 4.80 5.00 5.20 5.40 m/z 69.10 33.86%

5000 59 27 15 31 53 1′1-111111171 67, ,Ininuiiiiipiiiliurj mid rhja TTh 86 Arp miz—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4.80 5.00 5.20 5.40 4.60

00248.D SCAN508.M Fri Jan 25 10:26:10 2002 Page 8

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