GCMS analysis results for sample AE00248, Jan 2002

NYC 9/11 Public Portal Document Library searen compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN24\00248.D Vial: 4 • Acq On : 24 Jan 2002 5:27 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \ SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Formamide, N-(cyanomethyl)- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

4.85 0.15 ug/L 75814 1,4-Dichlorobenzene-d4 9.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Formamide, N-(cyanomethyl)- 84 C3H4N2O 005018-27-9 17 2 2-Pentyn-l-ol 84 C5H80 006261-22-9 16 3 2-Pentyn-l-ol 84 C5H80 006261-22-9 12 4 (E)-1-Propenylaziridine $$ Aziri... 83 C5H9N 080839-91-4 9 Abundance Scan 129 (4.847 min): 00248.D (-) m/z 83.95 100.00% 84 55 39 59 5000

1**+(‘‘I*"I r i i 114* 44 50 69 4.40 4.60 4.80 5.00 5.20

mz-> .1/117747 ' • I ■ ■'' i ■ ■ ■ ■ i ■ ■ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 i1 • • ■ i ■ ■ 11 ■ ■ ■ • i''' • i1 ■ i ■ ■ * ‘ i ■ • m/z 55.10 70.90% Abundance #3103: Formamide, N-(cyanomethyl)- 29

84 55 5000 i ■ ■ ■ ■ i ■ 1 I 1 1 4.40 4.60 4.80 5.00 5.20 40 m/z 59.00 55.24% 36 45 *H — 11 ■111 ITT niz-> 20 25 3035404550556065 70 7580 85 90 Abundance #3292:2-Pentyn-1-ol 39 55 / 4.40 4.60 AA 4.80 5.00 5.20 5000 83 m/z 39.10 55.18% 27 51 65

miz-> 20 “ i •'1' i ■ 25 • ■ i' ■ ■ ■ i ■' 30 35 40 45 50 55 ..... H^, ...... 60 65 70 75 80 85 90 11" 1' i ■ ■

Abundance #3291:2-Pentyn-1-ol ■ MA..,.. 39 55 4.40 4.60 4.80 5.00 5.20 m/z 41.10 48.25% 83 5000 27 44 51 66

/z—> " i' ■ ■11 ■ 20 25 mPPP 48— 30 35 40 45 50 55 m I, 60 65 70 75 80 85 90 •i *■ AA4Aoa 4.40 4.60 4.80 5.00 5.20

00248.D SCAN508.M Fri Jan 25 10:26:10 2002 Page 7

NYC-WTC_000050568