GCMS analysis results for sample AE00248, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN24\00248.D Vial: 4 Acq On : 24 Jan 2002 5:27 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1.. .\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 3-Penten-2-ol $$ .alpha.,.g... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 5.71 0.19 ug/L 93791 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Penten-2-ol $$ .alpha.,.gamma... 86 C5H10O 001569-50-2 64 2 3-Penten-2-ol 86 C5H10O 001569-50-2 64 3 3-PENTEN-2-OL, (Z)- 86 C5H10O 024652-50-4 64 4 1,6-Heptadien-4-ol 112 C7H120 002883-45-6 59 Abundance Scan 205 (5.714 min): 00248.D (-) m/z 43.10 100.00% 43 71 _ 17 1 _ 1 . I y 1 . 1 5000 39

53 58 — 84 5.40 5.60 5.80 6.00

niz-> ■■ i ■■■■i• ■' ■ i ‘

20 25 ■ i■11'I ' 4 30 35 40 45 50 55 60 65 70 75 80 85 — 90 95 m/z 71.10 99.88% Abundance #4047:3-Penten-2-ol $5 .alpha., gamma.-Dimethylallyl alco... 43 71

5000 39 TI 27 53 5.40 5.60 5.80 6.00 67 m/z 41.10 92.19% 58 86

niz-s 20 25 ... hai 30 35 40 45 49 ■ ‘ i1 ■ 50 -1-2111—63118 55 60 65 ‘I *mmmP 70 75 80 85 90 95 Abundance #4046:3-Penten-2-ol 71 43 - p Ai A r 5.40 5.60 5.80 6.00 5000 39 m/z 39.10 49.92% 53 67

L 27 58 86

niz—> 20 ■ ■ i ■" ■ i ■ g ■ ■ i ■'. ■ i'' ■ 30 35 40 1t1T - 45 50 55 60 65 +70 75 80 85 90 95 Abundance #4208:3-PENTEN-2-OL, (Z)- ■ ■ • i ' ■ 71 5.40 5.60 5.80 6.00 43 m/z 69.10 41.22%

5000 39 53 67 27 58 86

/z—> TTTTTTT ’ * i * * “ i ‘ 20 25 30 35 40 H 45 ‘ 5011 aal .. . PTpT — 55 60 65 70 75 80 85 90 95 T ............... ............................ 5.40 5.60 5.80 6.00

00248.D SCAN508.M Fri Jan 25 10:26:10 2002 Page 9

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