GCMS analysis results for sample AE00248, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN24\00248.D Vial: 4 Acq On : 24 Jan 2002 5:27 pm Operator: .Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 3-(CYCLOHEX-3’-EN-YL)PROPAN... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

5.89 4.24 ug/L 2115810 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 2 Acetic acid, 3-El,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 Silane, tetramethyl- $$ Tetramet... 88 C4H12Si 000075-76-3 28 4 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 Abundance Scan 220 (5.885 min): 00248.D (-) m/z 73.10 100.00% 73

5000 43

,11... 87 103............................. - 55 > i i'i'i'I'i > 11 ri'i 111 ■ 11 I'm 111 n 1111.11.. 11. h . । r... j।।. TT _ U ...... m/z 5.60 5.80 43.10 6.00 6.20 24.99% mfa-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180

1 Abundance #36138:3-(CYCLOHEX-3‘-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 ' ■ i • ‘ 1Y f ■ ■ ■ 5.60 5.80 6.00 6.20 43 m/z 41.10 9.28% 27 87 113 TTTTTT . i '55. i ' ■ ' '.i ■ T, | I'. । .... । . ...t > । । .t। 174 I । .. 1 . । .... | I miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3Jdioxolan-2-ylpropyl ester 73 5.60 5.80 6.00 6.20 5000 m/z 45.10 9.26%

43 5527 87 I Ip 113 174 mmppt 1’1111117111 111001000115000/—002/—0010010m18 mfz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4812: Silane, tetramethyl- $$ Tetramethylsilane $$ (CH3)4... 188 *•]•••• 73 5.60 5.80 6.00 6.20 m/z 71.10 6.35%

5000

n/z—> 15 1 31 45 11,55,. 88 '11 “ " I “ “ I “ 1'11 m | > 1 i 11 > 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 111 I it | 1 11 ■ 11 ।111 .AL.. 5.60 5.80 6.00 6.20

00248.D SCAN508.M Fri Jan 25 10:26:10 2002 Page 10

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