GCMS analysis results for sample AE00616, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02JAN29\00616.D Vial: 5 Acq On : 29 Jan 2002 5:59 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************** * * *** k * k * * * Peak Number 3 3-(CYCLOHEX-3'-EN-YL)PROPAN. .. Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 3.29 ug/L 1804940 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

13-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 25 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 220 (5.885 min): 00616.D (-) m/ z 73.10 100.00% 73

5000

43 . ....... ....... . I I 55 — 5.60 5.80 6.00 6.20 IPP 1''i'■' ■ i'''' i ■i'' ■' i' ■'' i' " ' r ''' i ■ " r i■1''i1 ■ m/z 43.10 24.00% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 70

5000 d—nn—TTmm0—uk33 5.60 5.80 6.00 6.20 43 m/z 45.10 9.24% 27 TIuu—mnuot 55..... ,, Ir ri87’ I ' H । ' 1 | r< ‘‘It 113 174 i ’ " ' i " " i • " ’ i ■ ■ ■ ■ i' " ' r ■ ■ ■ i' " ' i ■ ■ " i1 " ' i' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 70 • ■ • ■ । । • "i > > ■ ■ n i । । । . 5.60 5.80 6.00 6.20 5000 m/z 41.10 9.10% 43 27 55 87 113 174 TT ■ • i' ■1 ■ i1 T++ i" " 1‘"11111011111111171017111171111111T m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4814: Silane, tetramethyl- -P r { , ... I_ 1—- 73 5.60 5.80 6.00 6.20 m/z 71.10 6.50% 5000

45 15 | 53 | 88 TTTTTITTTTTTTTHTTTTTTTTT 1‘nuu‘00nn—un‘n————nmumDT—10nu m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

0616.D SCAN508.M Wed Jan 30 09:02:26 2002 Page 5

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