Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00466 conducted on January 18, 2002.
NYC-WTC_000051263–000051282Folder label: “GCMS X 1/8/02 A 1/10/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\5973N\02JAN10\00473.D Vial: 8 Acq On 10 Jan 2002 8:36 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 3-(CYCLOHEX-3'-EN-YL)PROPAN. .. Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
5.89 5.11 ug/L 1664760 1,4-Dichlorobenzene-d4 9.71
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 36 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 220 (5,885 min): 00473.D (-) m/z 73.10 100.00% 7
5000 43 5.60 5.80 6.00 6.20 0 i ■ ■ ■ ■ i ,1155.... , 11I-*mmm900TDTTUITTWTTT , 87 103 m/z 43.10 23.80% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1 -p... 70
5000 5.60 5.80 6.00 6.20 43 m/z 45.10 8.79% 27 55 87 113 174 01------- ' i ■ ■ " i " '1, 1I 1 ’ 1 1 | 1 1 111 | 1 1 1 ITFTIrgei i i | I I I I | I . I r | . . t r( i ! i .. 1 . m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 70 5.60 5.80 6.00 6.20 5000 m/z 41.10 8.67% 43 27 55 , 87 113 174 0- TTTT Tmmmm TWONuO'TTT HP i " " r "' i' " 11' n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 1 50 160 170 180 Abundance #4814: Silane, tetramethyl- _ _ ''I 111 1 70 5.60 5.80 6.00 6.20 m/z 71.10 6.21%
5000
45 15 m/z-> 0 TPP " ' 11‘‘al...... I 53 4—88 11" 1111" I" 1111 " 11" " i'1" r " ' i " " r 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20
30473.D SCAN508.M Fri Jan 11 10:09:08 2002 Page 3
NYC-WTC_000051269
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NYC-WTC_000052147
Laboratory report showing GCMS analysis of sample AE00832 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052088
Laboratory report showing GCMS analysis of sample AE00839 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052205
Instrument output file from GCMS analysis using method SCAN508 showing response for deuterated internal standards.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051605
Laboratory report showing GCMS analysis results for sample AE00614 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049957
Laboratory report showing GCMS analysis of sample AD31639 including unknown compounds and surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052187
Laboratory report showing GCMS analysis of sample AE00838 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050577
Laboratory report listing unknown compounds and surrogate recovery for sample AE00249 analyzed on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052069
Laboratory report showing GCMS analysis of sample AE00833 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009946
Analytical results for sample AE01507 analyzed via GCMS on March 4, 2002, including surrogate recovery data.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010126
GCMS laboratory results for sample AE01638 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003981
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018830
GCMS report for sample AD28861 showing detection of unknown compounds and surrogate recovery data.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000051152
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000051153
Document header page containing identification codes and metadata for GCMS files processed in early January 2002.
Filed in the same folder
NYC-WTC_000051156
Laboratory report detailing GCMS analysis of sample AE00327 for volatile organic compounds on January 10-11, 2002.
Filed in the same folder
NYC-WTC_000051165
Laboratory report showing GCMS analysis of reference standards used for calibration during January 10-11, 2002 testing.
Filed in the same folder
NYC-WTC_000051179
Laboratory report documenting GCMS blank analysis to verify system cleanliness during January 10-11, 2002 testing.
Filed in the same folder