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← Document results/DEP Box 28/GCMS X 1/8/02 A 1/11/02
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GCMS results for sample AE00329, Jan 24 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00329 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051485–000051499

Folder label: “GCMS X 1/8/02 A 1/11/02”

←Page 9 of 15→
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN11\00329.D Vial: 3 Acq On : 11 Jan 2002 3:46 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

5.89 4.81 ug/L 1467880 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

13-(CYCLOHEX-3'-EN-YL)PROPANOL 174 $$... C8H14O4 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 Silane, tetramethyl- $$ Tetramet... 88 C4H12Si 000075-76-3 28 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 220 (5.885 min): 00329.D (-) m/ z 73.10 100.00% 73

5000 43 5.60 5.80 6.00 6.20 O-TT -l 55 ■ i ■ ‘‘I " 111 87 103 m/z 43.10 23.47%

L m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 r1T1‘ 5.60 Pr 5.80 6.00 6.20 r-r-T-r-r-r-r-

43 m/ z 45.10 9.48% 27

L 87 113 174 0 PT 55 ■ I ' i ■' " i " ' 'T1 i' " ' r ' " i' " ' i i'1 ■' i1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 70 ' 1 , I ' ' ' I1 1 111* i 5.60 5.80 6 00 6.20 5000 m/ z 41.10 9.27%

43 27 55 87 113 174 0 " i111111i1"11'1 11" " r " > , i'i 1''' i11" i"1 ■ ........... I ’ * ’' I'''11' " 11'1111'1'11' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4812: Silane, tetramethyl- $$ Tetramethylsilane $$ (CH3)4... 1 ' i ' ■ TI I"'"1'1 ' 70 5.60 5.80 6.00 6.20 m/z 71.10 6.59%

5000

45 15 0 31 | 55 THDt 11'u I ‘ 488 ' 11 " ‘ I' "' 1111' I n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

00329.D SCAN508.M Mon Jan 14 10:46:47 2002 Page 5

NYC-WTC_000051493

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NYC-WTC_000051493Source: NYC Law Department, mirrored locally

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