GCMS results for sample AE00329, Jan 24 2002

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Laboratory report showing GCMS analysis of sample AE00329 with surrogate recovery data on January 24, 2002.

NYC-WTC_000051485–000051499

Folder label: “GCMS X 1/8/02 A 1/11/02”

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Data File : C:\MSDCHEM\1\5973N\02JAN11\00329.D Vial: 3 Acq On : 11 Jan 2002 3:46 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 2 3-hydroxy-4,4-dimethyl .gam... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 5.01 0.13 ug/L 40707 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-hydroxy-4,4-dimethyl .gamma. B... 130 C6H10O3 052126-90-6 42 2 2-Butenoic acid, 2-methoxy-, met.. 130 C6H10O3 056009-29-1 36 3 Butane, 2-bromo-2-methyl- $$ ter... 150 CSHllBr 000507-36-8 28 4 Hexane, 3,3,4-trimethyl- (CAS) $... 128 C9H20 016747-31-2 9 Abundance Scan 143 (5.006 min): 00329.D (-) m/z 43.10 100.00% 43 71

5000 59 / N । A.. • 1 । ■ > 207 4.60 4.80 5.00 5.20 5.40 l, l ., l as ' I' 11.1.... 1.... 1.... 1.... 1.... 11.... 1.... 1.... 1.... 1.... 1.... I 1... 0 " i" " r " ■ i' m/ z 71.10 96.31% m/z-> Abundance 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 #26149: 3-hydroxy-4,4-dimethyl .gamma. Butanolactone $$ Pa... ft 43 71

5000 4.60 4.80 —4 5.00 1'T'’'।|।। 5.20 5.40 57 m/ z 41.10 53.46% 31 0 ............ I.... Illll,.. .1.11,,, >1, !■................................................ ..................... " I " " r " ' I " " 111' ■ I ■ • 111 ■ ■ < 11....... 11 r 111111111 < i HI > 1111111111 | ■.. | ■.. | I. n I >.. |., > > |... |. m/z-> 10 20 30 40 50 60 70 80 90 10011012013014015016017018019020021 0 Abundance #26065: 2-Butenoic acid, 2-methoxy-, methyl ester, (E)- 43 71 1 1 i ' ‘‘ 1 i 1 1 4.60 4.80 5.00 5.20 5.40 5000 27 m/ z 69.10 44.98% 57 130 0 m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #45652: Butane, 2-bromo-2-methyl- $$ tert-Amyl bromide $$ ... 43 71 4.60 4.80 5.00 5.20 5.40 m/ z 59.10 34.71%

5000 27 55

/z-> 15 0 "i "'"i11 "■ ।1 + .. ,... , ........... 121......................... 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 A../).... ... 4.60 4.80 5.00 5.20 5.40

00329.D SCAN508.M Mon Jan 14 10:46:46 2002 Page 4

NYC-WTC_000051492

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GCMS results for sample AE00321, Jan 24 2002 · Box DEP Box 28

NYC-WTC_000051394

Laboratory report showing GCMS analysis of sample AE00321 with surrogate recovery data on January 24, 2002.

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