GCMS results for sample AE00329, Jan 24 2002

NYC 9/11 Public Portal Document

Llprary searcn compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN11\00329.D Vial: 3 Acq On : 11 Jan 2002 3:46 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 4-Pentenal (CAS) $$ 4-Pente... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 4.86 0.14 ug/L 42616 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-Pentenal (CAS) $$ 4-Pentenal- 84 C5H8O 002100-17-6 9 2 1-Hexene, 6-bromo- 162 C6HllBr 002695-47-8 9 3 2-Pentyn-1-ol 84 C5H80 006261-22-9 9 4 1-PROPENYL-AZIRIDINE 83 C5H9N 000000-00-0 7 Abundance Scan 130 (4.858 min): 00329.D (-) m/z 84.00 100.00% 84 55

5000 41 W 1 1

4.60 i 1 1 ■ ■

4 80 i ■ ■

5.00 5.20 77 0 > । >. ■. । ■ ■'i'‘■■।■ ■''। ■ ■ ■11■ T’I——291’’’’0’009B"uu’’T m/ z 55.10 75.97% m/z-> 20 30 40 50' 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #3208: 4-Pentenal (CAS) $$ 4-Pentenal- 41 55

5000 । । ■ 1 I 1 1 '■ । I 460 4.80 levin 5.00 5.20 . 83 m/z 41.10 57.36% 69

m/z-> O' 111111111' । ■ 20 30 40 +4 60 70 80 90 100 110 120 130 140 150 160 170 50 |....... I ........ . .............. ..................... .............. ......... ..................

Abundance #61496: 1-Hexene, 6-bromo- 41 55 M - 83 4.60 4.80 5.00 5.20 5000 m/z 39.10 54.37% 27 67

A m/z-> o TTTTT 20 30 40 □ 50 10TmIUPTIITTTTUTTLTTTITTIT’ ■ • i ■ ■' ■ i ■ ■ • > । 60 70 80 90 100 110 120 130 140 150 160 170 136 162

Abundance #3292: 2-Pentyn-1-ol 39 4.60 4.80 5.00 5.20 m/z 83.10 50.70% 83 5000 27

0 ■ i ■'' ■ i ■ ■ IT i'''' r ■'' i'' ■ ■ I ■f ■ 1 i 1 1 1 1 r' 1 ' । । । । । । । । 1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 4 60 4.80 5.00 5.20

00329.D SCAN508.M Mon Jan 14 10:46:46 2002 Page 3

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