GCMS analysis results for sample AE00473, Jan 18 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN10\00366.D Vial: 2 Acq On 10 Jan 2002 3:39 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 1 2-Pentenal, (E)- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 4.84 0.23 ug/L 73657 1,4-Dichlorobenzene-d4 9.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentenal, (E)- 84 C5H80 001576-87-0 33 2 l-Propenylaziridine 83 C5H9N 000000-00-0 25 3 1-PROPENYL-AZIRIDINE 83 C5H9N 000000-00-0 25 4 1-Hexene, 6-bromo-____________________ 162 C6HllBr 002695-47-8 17 Abundance Scan 128 (4.835 min): 00366.D (-) m/ z 84.00 1 00.00% 84 55 59 41 5000

51 4.404.60 4.80 5.00 5.20 ot ' ■ i ■ « | 1 > r ■ f r ■ 1 r । "TTTTT । ■ ■ • ■ ।1 ■ ■ ■ ।1 ■ i1 ■1' । ■ m/ z 55.10 75.35% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #3201: 2-Pentenal, (E)- 55 27 39 84 5000 4.40 4.60 4.80 5.00 5.20 m/z 59.10 70.34% 66 51

m/z-> Ol ■' i'' 20 +35+I"T -PPPPP 25 30 35 40 45 50 55 60 65 i ■ ■1 ■ । ■111111 1 “ • l ■ ■ ■ ■ I ‘ 70 75 ' l 1 ■ 80 I 1 ' 1 ' I ■ ' 85 90 Abundance #3036: 1-Propenylaziridine 41 55 83 A./M r .4 4.40 460 4.80 5.00 5.20 5000 27 m/ z 41.10 61.95%

m/z-> Abundance ol ' 11 ■111 20 "TFT ■ • > i > । ITI'111111 TII" 1'' i 11 ■ i11 ■111'' ■ IT 25 30 35 40 45 50 55 60 65 70 75 80 #3059:1-PROPENYL-AZIRIDINE 41 55 68 80

83 +PTTT 85 90

4.40 m/ z 14.60 4.80 39.10 5.00 5.20 57.05%

n/z-> 5000

0 20 25 27

■ ■ i • ■ ■ ■ i ■ ■ 30 35 40 m ill....... ll.... 45 50 55 60 65 68

70 80 111 ‘' 1 1' 75 80 Ip" ■ I • r 85 90 4.40 4 60 N.. 4.80 5.00 5.20

30366.D SCAN508.M Fri Jan 11 10:08:24 2002 Page 3

NYC-WTC_000051258