GCMS analysis results for sample AE00833, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN31\00833.D Vial: 1 Acq On : 31 Jan 2002 2 :42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 1-Propenylaziridine Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 4.88 0.05 ug/L 26394 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Propenylaziridine 83 C5H9N 000000-00-0 10 2 (E)-1-Propenylaziridine $$ Aziri... 83 C5H9N 080839-91-4 10 3 1-PROPENYL-AZIRIDINE 83 C5H9N 000000-00-0 10 4 Formamide, N- (cyanomethyl) -84 C3H4N20 005018-27-9 9 Abundance Scan 132 (4.881 min): 00833.D (-) m/ z 84.00 100.00% 5.5 84

5000 41

49 Ml w MAV 44 4.60 4.80 5.00 5.20 01 - IUt ■' i ■ ■ ■ ■ i ■ • ■ ■ i ■ ■' ■ i' ■ i ‘ ■ 1 i ■ ■ m/z 55.10 90.59% n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #3036:1 -Propenylaziridine 41 55 83

5000 27 11,1 Tr 1 1 1 । 11 ' 4.60 4.80 5.00 5.20 m/ z 41.10 70.46% 01 ■ ■ i ■' ■ ■ i ' ' i ' ' ' ■ i'1 ' ' i ' '' ' i1 ' 1‘I’ mmmTH 68 80 11 > > ■ * । ■1 a m/z--> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #3037: (E)-1-Propenylaziridine$$ Aziridine, 1-(1-propenyl... 41 55 83

4.60 4.80 5.00 5.20 1 5000 27 m/z 83.10 70.13%

68 52 1 ■n/z-> Ol ' 11 1 1 1 1 I 20 25 '' i 1 ■ '' i '' 30 35 ‘dt 40 ..... 111 ■ ■ i ■ ■ ■ ■ । ■ l i ■ i ■ ■ ■ ■ ।

45 50 55 60 65 70 75 80 85 90 ‘ 11 11 ■ ■ • ■ । ■

Abundance #3059:1-PROPENYL-AZIRIDINE ddddn/mmBmmmm 41 55 83 4.60 4.80 5.00 5.20 m/z 39.10 41.58%

5000 27 68

m/z-> 0 ‘1′21111 20 25 ' ■ 1111' i'1 30 35 40 mm III...... Il, 45 50 55 60 65 '' T* 70 75 80 80 11111 । [ > > 85 90 ■ ■ । > ■ • < । 4.60 4.80 ■ 1 1 I"1 1 11 1 ' 1 5.00 5.20

00833.D SCAN508.M Fri Feb 01 09:18:58 2002 Page 6

NYC-WTC_000052078