GCMS calibration analysis results, DEP Labs, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB21\0123B.D Vial: 1 Acq On : 21 Feb 2002 10:46 am Operator: Sample : lab blank 1/23 Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C: \MSDCHEM\1 . . . \HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 6 2-METHYL-3,3-D2-AZIRIDINE Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 9.90 0.06 ug/L 28328 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-METHYL-3,3-D2-AZIRIDINE 59 C3H5D2N 030691-55-5 5 2 1-Propanamine (CAS) $$ n-Propyla... 59 C3H9N 000107-10-8 4 3 1-Propanamine 59 C3H9N 000107-10-8 4 4 Propanoic acid, 2-hydroxy-2-meth... 104 C4H803 000594-61-6 4 Abundance Scan 578 (9.899 min): 0123B.D (-) m/ z 59.00 100.00% 59

5000 A. 144 M, , 45 73 9.60 9.80 10.00 10.20 o! 49 1 86 i■■■■i•■■■i■1'■i1 “ ■i■■■■11■■■i" ■■i m/ z 45.10 16.59% miz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #500:2-METHYL-3.3-D2-AZIRIDINE 29 58 M

5000- 9.60 9.80 10.00 10.20 42 m/ z 44.00 16.06% 26

n/z-> 0 mm - -HJ39 I ■ • ■ ■ i ■ ■ ■ ■ i ■" ■ i ■u ■ i1 “ • i ■ ■ ■ ■ i1 ■ ■ ■ ।

10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 J J Abundance #654:1-Propanamine (CAS) $$ n-Propylamine $$ Propylamine... 59 9.60 9.80 10.00 10.20 5000 42 m/z 43.10 15.69%

। 56 niz-> 45.51.4 0! “ i ■ “ • i “ “ i • ■111" “ 111" I" 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 |*■> ■ i * ■ > ■ i • * **i* ”11 ‘ ■ i1 *1 * i *'1 * i

Abundance #649:1-Propanamine ■ 'i■ '' 1 i ' rr i 1 1 r" 33 9.60 9.80 10.00 10.20 m/ z 73.00 12.19% 5000

59

n/z-> 17 0 ■11 ■ ■ ■' I'1'' l1 27 + 42 52 56,| tpHHp ■' i ■1 “ i' ■111 “111'111111" I " " IUUTut 1111 > 111 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 9.60 0/,./..... 9.80 10.00 10.20

0123B.D HP022102.M Mon Feb 25 10:54:37 2002 Page 8

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