GCMS analysis results for sample AE00843, Feb 4 2002

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Laboratory report showing GCMS analysis of sample AE00843 including surrogate recovery and unknown compounds.

NYC-WTC_000052128–000052146

Folder label: “GCMS X 1/11/02 A 1/31/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

- Data File : C:\MSDCHEM\1\5973N\02JAN31\00843.D Vial: 5 Acq On : 31 Jan 2002 6:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 2-Propanol, 1-(2-methoxypro... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

9.87 0.09 ug/L 47781 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 39 2 2-METHYL-3,3-D2-AZIRIDINE 59 C3H5D2N 030691-55-5 9 3 3-Octanol (CAS) $$ n-Octan-3-ol ... 130 C8H180 000589-98-0 9 4 Propanoic acid, 2-hydroxy-2-meth... 118 C5H10O3 002110-78-3 9 Abundance Scan 569 (9.870 min): 00843.D (-) m/ z 59.10 100.00% 59

5000

0 - 45 73 86 IV....4 80 ' ' 90 ' 100 110 120 104 130 m/z M. 9.60 9.80 45.10 ..M MA. 10.00 10.20 13.67% n/z-> 20 30 40 50 (60 70 Abundance #43942:2-Propanol, 1-(2-methoxypropoxy)- $$ 1-(2-Methoxyp... 59

5000 9.60* 1.1 9.80 10.00 10.20 m/z 42.10 12.95% 31 45 01 ■ i • • • • i • ■■■I1"'1............'I1! - ■ 73 104 130 1 I 1 1 1 1 I 1 1 1 1 I 1 1 1 1 1 1 1 ■ ' i 1 1 ■ ■ i ■ ■ ' 1 i 1 ' n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #500: 2-METHYL-3.3-D2-AZIRIDINE 23 58

r .......... .(..A.........................

9.60 9.80 10.00 10.20 5000 m/z 44.10 12.39%

42 0+ l l | ‘ । ■ • i ■ ■ ■ • i ■ ■ • ■ । ■ ■ ■ ■ [ ■ ■ ■ • i ■ • ■ ■ i ■ ■ ■ • i • Tl/Z--> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #26850: 3-Octanol (CAS) $$ n-Octan-3-ol $$ Ethylamylcarbin... 59 9.60 9.80 10.00 10.20 m/z 41.10 12.35%

5000 83

101 44 — I । । । । । । । ji । । 69 112 m/z-> 0 11 20 —30......4014..... 50 —TP 60 70 80 90 100 ■ ■ ।11 ■ ■ । ■ ■ ■ ■ ।■ 110 120 130 9.60 9.80 10.00 1020

00843.D SCAN508.M Fri Feb 01 09:19:28 2002 Page 10

NYC-WTC_000052141

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NYC-WTC_000052141Source: NYC Law Department, mirrored locally

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Laboratory report showing GCMS analysis of sample AE00840 including surrogate recovery and unknown compounds.

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