GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB05\30644A.D Vial: 1 Acq On 5 Feb 2002 2:56 pm Operator: Sample : 508 scan; re-ext Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 2-Propanol, 1-(2-methoxypro... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 9.85 0.19 ug/L 138047 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 78 2 PROPYLENE GLYCOL TRIMER 1 174 C9H18O3 000000-00-0 9 3 .beta.-Fluoroallyl ethyl ether 104 C5H9FO 000000-00-0 7 4 2-METHYL-3,3-D2-AZIRIDINE 59 C3H5D2N 030691-55-5 ,7 Abundance Scan 567 (9.847 min): 30644A.D (-) m/ z 59.10 100.0*0% 59

5000

— 45 73 86 104 N 1'1 r11 1 1 i 1 1 1 1 i 9.60 9.80 10.00 10.20 0 L ............ | I 1 I > I 1 1 1 1 I ‘11 ■ 1 I 1 1 ■ 1 I ' > ■ 1 I 1 ' m/ z 45.10 11.17%

W i 1 ' ' ■ i ■ ■ ■ ' i nz-> 20 30 40 50 60 70 80l 90 100 110 120 130 Abundance #43942:2-Propanol, 1 -(2-methoxypropoxy)- $$ 1-(2-Methoxyp... 59

5000 ■ ■ l > ■

9.60 9.80 10.00 10.20 m/z 41.10 9.90% 31 45 O1^ — 0I|I,..... lasi 73............. 104 ........... 130 ■ i 1 ' ■ 1 i ' ' ■ ■ i ■ ■ ■ 1 i ■ 1 ■ ■ i ■ r ■ ■ 1 1 ' 1 ' i ' 1 m&-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #78532: PROPYLENE GLYCOL TRIMER 1 59 MA,., 9.60 9.80 10.00 10.20 5000 41 m/z 43.10 9.65% 103

0- ......... I. —50r —l- 73 ' I > • 117IIIIII 87 i » • ‘ >l'> 1TPPII 130 N A m/z-> 20 30 40 60 80 90 70 100 110 120 130 Abundance #10165: .beta.-Fluoroallyl ethyl ether 59 9,60 9,80 10,00 10.20 m/z 73.10 8.97%

5000 45 76 27

m/z- > 33 0 ' i 1 ' 1 ■ i ■ ■ 1 ' i ■ 20 30 40 Hi 1 ■ 50 r.... I 60 70 89 104 ' i ■ ■ ''i 1■ ■1 i ■1■ ‘i ■1■ 1 I 1 1 1 1 I 1 1

80 90 100 110 120 130 AW 9.60 9.80 10.00 10.20

30644A.D SCAN508.M Fri Feb 22 11:44:24 2002 Page 10

NYC-WTC_000004909

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