GCMS analysis results for sample AE00843, Feb 4 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00843 .D Vial: 5 Acq On : 31 Jan 2002 6:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 2,3,4,5-Tetrahydropyridazine Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

11.27 0.08 ug/L 45385 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,3,4,5-Tetrahydropyridazine 2 2(3H)-Furanone, dihydro- (CAS) $... 84 C4H8N2 86 C4H602 000694-06-4 9 000096-48-0 9 / 30 3 2,3,4,5-Tetrahydropyridazine 84 C4H8N2 000694-06-4 7 1 SA—

X 4 2(3H)-Furanone, dihydro- (CAS) $... 86 C4H602 000096-48-0 7 Abundance Scan 692 (11.274 min): 00843.D (-) m/z 84.05 100.00% 84 126 42 5000

11.00 11.20 11.40 11.60 0'i 111 49 m/z 126.10 68.23% ■ i 1 ■ ■ ■ i ■ ■ ■ ■ i ■ 1 ' ' i '

n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3177: 2,3.4,5-Tetrahydropyridazine 84 N

29 5000 55 41 11.00 11.20 11.40 11.60 69 m/z 42.10 55.81% 0- ■ > i ■ ■ ■ • i ■ • "IT ■ i • ■ ■ ■ i ■ ■ ■ • i ■

Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3838: 2(3H)-Furanone, dihydro- (CAS) $$ Butyrolactone $$ ... 42

86 11.00 11.20 11.40 11.60 29 m/z 44.10 52.41% 5000

tnM 56

n/z-> 0- —+ 10 20 30 40 50 TIT 1......... 60 70 80 90 100 .... 110 120 130 y Abundance #3178: 2,3,4,5-Tetrahydropyridazine 84 11.00 11.20 11.40 11.60 m/z 85.90 36.24% 29 I L 5000 55 AA 42 69 — 0 .. । ... ■ । • • | . 11 i ■ i > ■ ■ • i • T"T 1 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 11.00 11.20 11.40 11.60

00843.D SCAN508.M Fri Feb 01 09:19:28 2002 Page 11

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