GCMS calibration analysis results, DEP Labs, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

* Data File : C:\MSDCHEM\l\5973N\02FEB21\0123B.D Vial: 1 Acq On : 21 Feb 2002 10:46 am Operator: Sample : lab blank 1/23 Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C: \DATABASE\WILEY7N . L ******************************************************************** * Peak Number 7 2,5-Diamino-6-methyl-4-pyri... Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 13.38 0.04 ug/L 23631 Naphthalene-d8 13.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2,5-Diamino-6-methyl-4-pyrimidinol 140 C5H8N4O 000000-00-0 45 2 2,5-Cyclohexadiene-1,4-dione, 2,... 140 C6H404 000615-94-1 40 3 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 40 4 2-Methoxy-3-hydrazinyl-pyrazine 140 C5H8N40 000000-00-0 38 Abundance Scan 886 (13.376 min): 0123B.D (-) m/z 140.00 100.00% 140

5000

70 86 96 1300 13.20 13.40 13.60 13.80 0! ■....,54..,. ------- 1.. ■ ■ ■ ‘ i m/z 69.90 20.35% miz-> :30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35088:2,5-Diamino-6-methyl-4-pyrimidinol VO

5000 .. 1 1 1 1 1 ■ ■ ' i ■ 13.00 13.20 13.40 13.60 13.80 70 m/z 96.00 13.08% 42 I 54 95 111 123 ol -PP — i 11 ■11 miz-> :30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35123:2,5-Cyclohexadiene-1,4-dione, 2,5-dihydroxy- hO • i * * * ■ i * * * > i * ■ » * । * 13.00 13.20 13.40 13.60 13.80 42 5000 m/z 141.10 12.09% 69

53 84 94 112 01— ■ ■ i ■ 1 ■ ■ i ■ ■ op i, , , , , iz-> :30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... ■ i ■ ■ 1 1 i ■ ‘ ■ ■ i • ■ ■ ■ i ■ 140 13.00 13.20 13.40 13.60 13.80 m/ Z 44.10 10.62% / 5000

44 71 123

mfe-> 0 —30PP 40 50 60 II70 m 11 • ■ ■ ■ । 80 ■ 90 100 110 120 130 140 86 96 112 TdI 13.00 13.20 13.40 13.60 13.80

0123B.D HP022102.M Mon Feb 25 10:54:37 2002 Page 9

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