DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB26\02015.D Vial: 3 Acq On : 26 Feb 2002 11:57 am Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 6, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 9 Pyrimidinetetramine- $$ Pyr... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 13.38 0.05 ug/L 34657 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 72 2 Uracil, 5-ethyl- $$ 2,4(1H,3H)-P... 140 C6H8N2O2 004212-49-1 50 3 2-Methoxy-3-hydrazinyl-pyrazine 140 C5H8N4O 000000-00-0 43 4 2,5-Cyclohexadiene-1,4-dione, 2,... 140 C6H404 000615-94-1 39 Abundance Scan 886 (13.376 min): 02015.D (-) m/z 140.00 100.00% 140

5000

70 86 94 108 13.00 13.20 13.40 13.60 13.80 44 ' I I | ‘ I I . ! I , I I | . . . I I I ! I I ! , I m/ z 94.10 12.72% 0b 11I m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... 140

5000 13.00 13.20 13.40 13.60 13.80 44 71 123 m/ z 69.90 11.59% 86 96 112

m/z-> 0b 301 - 40 ......... 50 60 Il 70 80 90 * | 100 110 120 130 140 ■ ' ■ 1 i

Abundance #35153: Uracil, 5-ethyl- $$ 2,4(1 H,3H)-Pyrimidinedione, 5-... 140 125 ' i 1 ‘ ' 1 i 1 ' ' ' i 1 ' 1 1 i ' 82 13.00 13.20 13.40 13.60 13.80 5000 m/z 96.00 9.99% | 54 68 96 | 111 ob 1 ' 1 1 1 1 1 I ' 1 ' ' I /‘onili 1 i'1 11II +Ttt TII m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35089: 2-Methoxy-3-hydrazinyl-pyrazine 140 13.00 13.20 13.40 13.60 13.80 m/z 141.10 9.67% 5000- 42 54 68

m/z-> O-TPT 30 40 ‘1* 50 1 1 i 1 1 60 70 m 80

80 90 95 .....108.... 1-]21I,. —L 100 110 120 130 140 1ii ' i ' ' ' ' i ' ' ' । I । 13.00 13.20 13.40 13.60 13.80 ■ I '

02015.D HP022102.M Wed Feb 27 08:34:25 2002 Page 11

NYC-WTC_000004559